1,7-Octadien-3-ol, acetate

Mass

MS-IW-3575          
1-vinyl-5-hexenyl acetate
C10H16O2            (Mass of molecular ion:    168)

   Source Temperature: 210 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      15.0       3.3
      27.0      11.6
      28.0       3.9
      29.0       8.4
      31.0       1.0
      39.0      18.2
      40.0       2.7
      41.0      25.4
      42.0       3.8
      43.0     100.0
      44.0       5.0
      45.0       1.9
      51.0       2.0
      52.0       1.3
      53.0       7.4
      54.0      46.1
      55.0      20.2
      56.0       2.3
      57.0      17.1
      58.0       4.5
      60.0       1.2
      61.0       1.7
      65.0       3.7
      66.0       9.4
      67.0      49.0
      68.0       6.2
      69.0       4.1
      70.0       7.2
      71.0       6.7
      72.0       6.3
      77.0       4.4
      78.0       4.2
      79.0      28.2
      80.0      18.8
      81.0       5.6
      82.0       6.3
      83.0       7.4
      84.0      13.9
      85.0       1.9
      91.0       4.0
      93.0      23.8
      94.0       2.5
      95.0       1.8
      97.0       5.3
      98.0       4.2
      99.0      24.4
     100.0       2.1
     107.0       2.6
     108.0      10.5
     109.0       2.9
     110.0       1.0
     111.0       7.6
     112.0       1.7
     113.0       1.0
     114.0       2.0
     125.0       2.6
     126.0       7.1
     127.0       1.0

Assign. Shift(ppm) A 5.771 B 5.767 C 5.24 D 5.232 E 5.156 F 5.007 G 4.956 J 2.06 K 2.056 L 1.62 M 1.43 J(A,F)=17.2HZ J(A,G)=10.5HZ J(A,J)=6.5HZ J(B,D)=17.3HZ J(B,E)=10.5HZ J(B,C)=6.5HZ

     Hz     ppm     Int.

   2322.51   5.812     96
   2316.16   5.796     55
   2312.01   5.786    132
   2305.18   5.768    149
   2301.64   5.760     34
   2298.83   5.753     94
   2294.80   5.743     95
   2288.33   5.726    103
   2103.39   5.264     32
   2099.98   5.255     79
   2098.75   5.252    143
   2097.53   5.249    143
   2090.94   5.232     60
   2090.09   5.230     66
   2088.99   5.228     39
   2082.64   5.212     99
   2081.30   5.208    125
   2080.08   5.205     69
   2066.89   5.172     77
   2065.80   5.170    124
   2064.58   5.166     65
   2056.52   5.146     72
   2055.30   5.143    113
   2054.08   5.140     72
   2011.72   5.034     37
   2010.13   5.030     82
   2008.18   5.025     93
   2006.59   5.021     46
   1994.63   4.991     34
   1993.04   4.987     75
   1991.09   4.983     84
   1989.50   4.979     43
   1987.67   4.974     46
   1986.45   4.971     86
   1985.35   4.968     65
   1984.38   4.966     73
   1983.15   4.963     40
   1977.42   4.948     41
   1976.20   4.945     79
   1975.10   4.943     61
   1974.24   4.940     67
   1973.02   4.937     37
    836.43   2.093     46
    834.72   2.089     38
    830.20   2.078     95
    829.10   2.075    120
    827.76   2.072     78
    826.78   2.069     62
    821.66   2.056   1000
    817.99   2.047     56
    816.28   2.043     51
    814.82   2.039     61
    813.48   2.036     42
    811.28   2.030     30
    666.99   1.669     39
    660.89   1.654     40
    659.79   1.651     36
    657.10   1.645     53
    654.05   1.637     54
    650.88   1.629     54
    650.02   1.627     48
    647.83   1.621     52
    644.90   1.614     43
    643.80   1.611     48
    641.60   1.606     43
    638.79   1.599     66
    632.69   1.584     48
    585.57   1.466     33
    580.69   1.453     31
    579.71   1.451     31
    578.49   1.448     44
    576.54   1.443     34
    573.12   1.435     60
    570.68   1.428     54
    569.09   1.424     36
    566.53   1.418     45
    564.94   1.414     36
    563.23   1.410     63
    561.89   1.406     31
    556.88   1.394     37
    555.79   1.391     34