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MassMS-IW-3474 3,4-dimethoxy-n-methylphenethylamine C11H17NO2 (Mass of molecular ion: 195)
Source Temperature: 220 °C Sample Temperature: 160 °C Reservoir, 75 eV
28.0 1.8 39.0 2.8 42.0 4.3 43.0 1.6 44.0 100.0 45.0 4.3 51.0 3.1 52.0 1.3 53.0 1.0 58.0 14.1 63.0 1.4 65.0 4.0 77.0 4.0 78.0 3.6 79.0 2.2 89.0 1.4 90.0 1.6 91.0 3.7 105.0 2.2 106.0 3.3 107.0 4.6 108.0 1.7 109.0 1.9 118.0 1.0 121.0 2.0 135.0 1.3 137.0 6.5 151.0 10.8 152.0 62.5 153.0 6.3 164.0 1.2 165.0 1.1 195.0 1.0
400 MHz in CDCl3
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1H NMR 399.65 MHz C11 H17 N O2 0.05 ml : 0.5 ml CDCl3 3,4-dimethoxy-N-methylphenethylamine 
Assign. Shift(ppm)
A 6.788 B 6.75 C 6.74 D *1 3.855 E *1 3.830 F 2.815 G 2.747 J 2.424 K 1.99
Hz ppm Int.2718.99 6.804 115 2714.23 6.792 34 2710.33 6.782 245 2698.12 6.752 93 2696.17 6.747 200 2694.34 6.742 231 2692.50 6.738 187 2689.58 6.730 107 2687.62 6.725 52 1540.65 3.855 974 1530.88 3.831 1000 1133.79 2.837 40 1132.20 2.833 44 1125.49 2.817 127 1119.26 2.801 117 1103.64 2.762 154 1097.53 2.747 179 1091.06 2.731 57 1089.11 2.726 53 968.99 2.425 667 794.92 1.990 55
liquid film
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