2-(Hydroxymethyl)piperidine

Mass

MS-NW-6721          
2-piperidinemethanol
C6H13NO             (Mass of molecular ion:    115)

   Source Temperature: 250 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      15.0       1.0
      18.0       1.1
      27.0       4.4
      28.0      11.1
      29.0       3.7
      30.0       9.7
      31.0       2.4
      39.0       3.6
      41.0       7.9
      42.0       6.1
      43.0       1.5
      44.0       1.2
      53.0       1.2
      54.0       2.4
      55.0       7.9
      56.0      19.3
      57.0       2.6
      59.0       1.1
      67.0       2.7
      68.0       2.0
      69.0       1.8
      72.0       1.1
      82.0       2.5
      84.0     100.0
      85.0       6.3
      96.0       1.1

Assign. Shift(ppm) A 3.6 B *1 3.529 C *1 3.377 D 3.070 E 2.63 F 2.61 G 1.791 J 1.610 K 1.540 L 1.42 M 1.35 N 1.113 J(B,C)=-10.7HZ J(B,E)=3.7HZ J(C,E)=8.3HZ J(F,J)=2.8HZ ASSIGNED BY H-H C0SY.

     Hz     ppm     Int.

   1418.46   3.550    701
   1414.79   3.541    736
   1407.71   3.523    959
   1404.05   3.514    951
   1358.40   3.399    940
   1350.22   3.379   1000
   1347.78   3.373    750
   1339.48   3.352    752
   1236.94   3.096    198
   1234.50   3.089    340
   1233.03   3.086    432
   1230.71   3.080    278
   1225.34   3.067    243
   1223.02   3.061    375
   1221.31   3.056    472
   1217.53   3.047    250
   1062.62   2.659    214
   1059.08   2.651    309
   1056.40   2.644    417
   1054.44   2.639    631
   1051.51   2.632    516
   1047.97   2.623    536
   1045.41   2.616    757
   1042.72   2.610    876
   1040.65   2.604    392
   1036.99   2.595    284
   1033.69   2.587    353
   1030.76   2.580    368
    724.85   1.814    303
    723.51   1.811    309
    721.56   1.806    285
    716.43   1.793    225
    712.65   1.784    294
    712.40   1.783    294
    710.57   1.778    269
    709.11   1.775    261
    704.47   1.763    110
    700.81   1.754     46
    649.41   1.625    293
    646.61   1.618    245
    643.92   1.612    190
    638.67   1.599    424
    636.96   1.594    476
    628.17   1.572    171
    624.63   1.563    353
    622.19   1.557    374
    617.55   1.546    176
    615.48   1.541    187
    611.45   1.530    387
    611.08   1.530    387
    610.72   1.529    387
    609.62   1.526    401
    608.03   1.522    364
    605.35   1.515    172
    600.71   1.504     75
    598.51   1.498     62
    597.90   1.497     62
    597.53   1.496     62
    596.80   1.494     61
    594.73   1.489     47
    593.38   1.485     47
    592.77   1.484     46
    589.84   1.476    118
    588.26   1.472     74
    586.06   1.467    160
    582.52   1.458    104
    577.15   1.445    244
    573.36   1.435    357
    569.82   1.426    222
    565.06   1.414    261
    564.45   1.413    254
    561.04   1.404    411
    557.50   1.395    355
    555.05   1.389    271
    553.96   1.387    296
    552.49   1.383    273
    549.68   1.376    357
    548.46   1.373    343
    546.14   1.367    513
    542.48   1.358    311
    537.23   1.345    236
    533.57   1.336    412
    529.91   1.326    245
    524.54   1.313    115
    520.87   1.304    168
    517.21   1.295     98
    463.99   1.161    209
    459.96   1.151    180
    455.93   1.141     61
    451.42   1.130    394
    448.73   1.123    278
    447.51   1.120    300
    440.19   1.102    368
    436.16   1.092    288
    431.64   1.081     60
    427.61   1.070    175
    425.42   1.065     79
    423.71   1.061    108