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MassMS-IW-9329 2-bromo-3-methylpyridine C6H6BrN (Mass of molecular ion: 171)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
26.0 1.3 27.0 1.7 28.0 1.2 37.0 2.8 38.0 5.6 39.0 17.5 40.0 1.7 41.0 1.9 45.5 1.4 50.0 2.1 51.0 2.6 52.0 1.9 61.0 1.1 62.0 1.9 63.0 6.2 64.0 7.9 65.0 49.3 66.0 5.0 84.5 1.0 85.5 1.7 90.0 1.5 91.0 8.4 92.0 100.0 93.0 7.2 171.0 34.8 172.0 3.1 173.0 34.1 174.0 2.5
400 MHz in CDCl3
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1H NMR 399.65 MHz C6 H6 Br N 0.05 ml : 0.5 ml CDCl3 2-bromo-3-methylpyridine 
Assign. Shift(ppm)
A 8.179 B 7.510 C 7.168 D 2.367
Hz ppm Int.3270.51 8.184 118 3267.09 8.175 117 3006.71 7.524 131 3005.74 7.521 129 2999.27 7.505 143 2998.29 7.503 139 2870.61 7.183 138 2865.84 7.171 141 2863.16 7.165 129 2858.40 7.153 119 945.92 2.367 1000
in CDCl3
liquid film
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