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3424-93-9

4-Methoxybenzamide

Product Name 4-Methoxybenzamide

CAS3424-93-9

MFC8H9NO2

MW151.16

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  • 3424-93-9_ms_1
    Mass 

    MS-NW-6702          
p-anisamide
C8H9NO2             (Mass of molecular ion:    151)


       Source Temperature: 260 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV


          15.0       1.4
      18.0       3.3
      27.0       1.4
      28.0       1.7
      29.0       1.0
      31.0       2.1
      37.0       1.5
      38.0       4.1
      39.0       4.1
      44.0       5.1
      45.0       1.0
      50.0       5.3
      51.0       4.3
      52.0       1.7
      53.0       2.1
      61.0       1.2
      62.0       2.7
      63.0       9.3
      64.0      10.1
      65.0       4.1
      74.0       2.6
      75.0       2.5
      76.0       3.5
      77.0      24.1
      78.0       2.9
      79.0       2.2
      80.0       1.7
      90.0       2.1
      91.0       1.2
      92.0      16.8
      93.0       1.8
     103.0       2.2
     104.0       1.3
     107.0      13.7
     108.0       2.8
     120.0       1.0
     122.0       1.1
     133.0       3.9
     134.0       1.1
     135.0     100.0
     136.0       9.3
     137.0       1.1
     151.0      56.0
     152.0       6.4

400 MHz in DMSO-d6

90 MHz in DMSO-d6

  • 3424-93-9_1hnmr_2

    1H NMR 399.65 MHz
    C8 H9 N O2 0.037 g : 0.5 ml DMSO-d6
    p-anisamide
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             7.887
      B     *1      7.88
      C     *1      7.24
      D             6.993
      E             3.813
  

         Hz     ppm     Int.


       3156.62   7.899    276
   3147.83   7.877    274
   2895.02   7.244     41
   2802.25   7.012     32
   2799.32   7.005    270
   2797.24   7.000     77
   2792.48   6.988     81
   2790.41   6.983    245
   2787.48   6.975     27
   1524.17   3.814   1000

  • 3424-93-9_1hnmr_0

    1H NMR 89.56 MHz
    C8 H9 N O2 0.043 g : 0.5 ml DMSO-d6
    p-anisamide
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             7.877
      B             7.19
      C             6.990
      D             3.812
  

         Hz     ppm     Int.


        713.44   7.967     23
    710.56   7.934    210
    708.44   7.911     67
    705.88   7.882     23
    705.50   7.878     23
    703.75   7.858     77
    701.56   7.834    259
    698.69   7.802     43
    632.75   7.066     29
    629.88   7.034    240
    627.69   7.009     62
    623.06   6.957     54
    620.94   6.934    181
    341.38   3.812   1000

in DMSO-d6

  • 3424-93-9_13cnmr_0

KBr disc

  • 3424-93-9_ir1_2

nujol mull

  • 3424-93-9_ir2_1

4880 A,200 M,powder

  • 3424-93-9_raman_0

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