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2,2'-ETHYLENEDIANILINE

Product Name 2,2'-ETHYLENEDIANILINE

CAS34124-14-6

MFC14H16N2

MW212.29

¹³CNMR

Mass

MS-IW-8135          
2,2'-ethylenedianiline
C14H16N2            (Mass of molecular ion:    212)

   Source Temperature: 130 °C
   Sample Temperature: 110 °C
   Direct, 75 eV

      30.0       1.3
      77.0       6.3
      78.0       1.7
      79.0       5.2
      91.0       1.2
     104.0       1.0
     106.0     100.0
     107.0       9.0
     118.0       2.0
     119.0       2.1
     194.0       1.6
     212.0      29.3
     213.0       4.7

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₄ H₁₆ N₂	0.039 g : 0.5 ml CDCl₃
2,2'-ethylenedianiline

    Assign.     Shift(ppm)

      A             7.04
      B             7.03
      C             6.733
      D             6.636
      E             3.53
      F             2.771

     Hz     ppm     Int.

   2819.21   7.055    281
   2817.50   7.050     80
   2815.67   7.046     40
   2811.52   7.035    382
   2809.81   7.031    152
   2803.96   7.017    148
   2802.37   7.013    109
   2698.73   6.753    127
   2697.51   6.750    141
   2691.41   6.735    208
   2690.19   6.732    233
   2683.96   6.716    107
   2682.74   6.713    111
   2656.62   6.648    187
   2655.88   6.646    172
   2655.27   6.644    152
   2648.80   6.628    177
   2647.71   6.626    146
   1409.30   3.527    272
   1107.42   2.771   1000

in CDCl3

KBr disc

nujol mull

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