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33884-43-4

2-(2-Bromoethyl)-1,3-dioxane

Product Name 2-(2-Bromoethyl)-1,3-dioxane

CAS33884-43-4

MFC6H11BrO2

MW195.05

More

  • 33884-43-4_ms
    Mass

    MS-NW-7374          
    2-(2-bromoethyl)-1,3-dioxane
    C6H11BrO2           (Mass of molecular ion:    194)
    

       Source Temperature: 200 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          26.0       2.6
          27.0      12.0
          28.0      15.5
          29.0      10.9
          31.0      21.4
          39.0       3.4
          41.0       9.1
          43.0       1.1
          55.0       2.3
          56.0       3.0
          57.0      13.9
          58.0       1.1
          59.0      14.0
          87.0     100.0
          88.0       4.9
         107.0       5.3
         108.0       1.0
         109.0       5.4
         135.0       3.9
         136.0       1.2
         137.0       4.2
         138.0       1.1
         193.0       5.0
         195.0       5.0
    

400 MHz in CDCl3

  • 33884-43-4_1hnmr

    1H NMR 399.65 MHz
    C6 H11 Br O2 0.05 ml : 0.5 ml CDCl3
    2-(2-bromoethyl)-1,3-dioxane
    ChemicalStructure
        Assign.     Shift(ppm)
    A 4.702 B 4.096 C 3.782 D 3.453 E 2.129 F 2.059 G 1.355

         Hz     ppm     Int.
    

       1884.28   4.715    226
       1879.27   4.703    434
       1874.15   4.690    232
       1646.48   4.120    197
       1645.14   4.117    254
       1643.92   4.114    128
       1641.48   4.108    206
       1640.14   4.104    262
       1638.79   4.101    130
       1635.86   4.094    123
       1634.64   4.091    285
       1633.30   4.087    260
       1630.98   4.082    142
       1629.64   4.078    291
       1628.30   4.075    246
       1524.66   3.815    214
       1523.07   3.812    173
       1522.09   3.809    235
       1520.63   3.805    133
       1514.04   3.789    119
       1512.08   3.784    334
       1509.89   3.779    339
       1508.30   3.775    154
       1501.71   3.758    103
       1500.24   3.754    199
       1499.27   3.752    158
       1497.68   3.748    193
       1387.33   3.472    536
       1380.37   3.454   1000
       1373.54   3.437    570
        860.47   2.154    343
        855.47   2.141    344
        853.64   2.136    632
        848.51   2.124    624
        846.68   2.119    388
        843.51   2.111     53
        841.67   2.107    394
        836.55   2.094     76
        834.11   2.088     98
        833.13   2.085     79
        829.10   2.075    168
        828.13   2.073    124
        824.10   2.063     89
        823.12   2.060     72
        821.66   2.056     65
        820.68   2.054    101
        816.53   2.044     98
        815.67   2.041    177
        811.52   2.031     54
        810.67   2.029     91
        808.23   2.023     52
        803.22   2.010     83
        798.22   1.998     41
        552.12   1.382     57
        550.78   1.379    105
        549.56   1.376    151
        548.22   1.372    192
        547.00   1.369    157
        545.65   1.366    115
        544.43   1.363     64
        538.70   1.348     57
        537.35   1.345    100
        536.13   1.342    140
        534.79   1.339    175
        533.57   1.336    139
        532.23   1.332    100
        530.88   1.329     54
    

in CDCl3

  • 33884-43-4_13cnmr

liquid film

  • 33884-43-4_ir1

  • 33884-43-4_raman