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Ethylene Glycol Bis(propionitrile) Ether

Product Name Ethylene Glycol Bis(propionitrile) Ether

CAS3386-87-6

MFC8H12N2O2

MW168.19

¹³CNMR

Mass

MS-NW-1107          
3,3'-(ethylenedioxy)dipropionitrile
C8H12N2O2           (Mass of molecular ion:    168)

   Source Temperature: 240 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV

      15.0       2.4
      18.0       1.2
      26.0       3.1
      27.0       8.5
      28.0       7.6
      29.0       4.5
      31.0      14.2
      40.0       1.4
      41.0       2.8
      42.0       1.7
      43.0       3.7
      44.0       2.7
      45.0      18.9
      52.0       3.0
      53.0       2.1
      54.0     100.0
      55.0       7.1
      57.0       1.4
      68.0       2.8
      70.0       1.5
      72.0       1.8
      84.0      41.4
      85.0       3.6
      97.0      11.8
      98.0      14.6
      99.0       3.6
     128.0       1.4
     138.0       1.6
     141.0       6.6

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₈ H₁₂ N₂ O₂	0.04 ml : 0.5 ml CDCl₃
3,3'-(ethylenedioxy)dipropionitrile

    Assign.     Shift(ppm)

      A             3.73
      B             3.687
      C             2.639

     Hz     ppm     Int.

    340.94   3.807    154
    334.44   3.735    351
    332.38   3.712     31
    330.19   3.687   1000
    328.44   3.668    231
    242.19   2.705    198
    236.06   2.636    369
    229.81   2.566    149

in CDCl3

CCl4 solution

liquid film

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