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MassMS-IW-0866 1-phenethylpiperidine C13H19N (Mass of molecular ion: 189)
Source Temperature: 210 °C Sample Temperature: 150 °C Reservoir, 75 eV
30.0 1.0 41.0 3.5 42.0 3.7 44.0 2.6 55.0 4.2 69.0 2.0 70.0 2.6 77.0 1.3 79.0 1.0 96.0 2.0 98.0 100.0 99.0 7.1 104.0 1.2 105.0 2.2
400 MHz in CDCl3
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1H NMR 399.65 MHz C13 H19 N 0.05 ml : 0.5 ml CDCl3 1-phenethylpiperidine 
Assign. Shift(ppm)
A 7.248 B 7.18 C 7.16 D 2.798 E 2.542 F 2.45 G 1.608 J 1.439
Hz ppm Int.2906.74 7.274 239 2905.76 7.271 379 2904.17 7.267 157 2899.17 7.255 645 2898.44 7.253 777 2897.46 7.250 582 2895.02 7.244 247 2893.19 7.240 299 2891.24 7.235 835 2886.47 7.223 41 2886.23 7.222 41 2875.00 7.194 600 2873.66 7.191 991 2873.29 7.190 1000 2871.09 7.185 271 2869.63 7.181 395 2867.80 7.176 455 2866.58 7.173 652 2865.97 7.172 552 2863.40 7.165 263 2861.33 7.160 480 2859.01 7.154 142 2855.59 7.146 124 2854.13 7.142 191 2852.78 7.139 104 1127.20 2.821 467 1121.58 2.807 315 1119.14 2.801 458 1115.36 2.791 322 1110.47 2.779 624 1023.93 2.563 834 1019.17 2.551 395 1018.55 2.549 414 1015.63 2.542 549 1014.65 2.539 526 1012.70 2.534 403 1007.20 2.521 588 978.52 2.449 491 654.91 1.639 281 649.29 1.625 648 643.43 1.610 912 637.82 1.596 811 632.32 1.583 357 586.18 1.467 130 579.96 1.452 275 574.58 1.438 327 568.85 1.424 193 563.35 1.410 79
in CDCl3
liquid film
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