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MassMS-NW-7147 2-(2-thienyl)pyridine C9H7NS (Mass of molecular ion: 161)
Source Temperature: 240 °C Sample Temperature: 180 °C Reservoir, 75 eV
26.0 1.3 27.0 1.5 28.0 2.1 37.0 1.2 38.0 2.2 39.0 7.1 45.0 6.9 50.0 5.1 51.0 9.2 52.0 4.6 57.0 1.3 58.0 3.8 58.5 2.5 61.0 1.1 62.0 2.2 63.0 5.3 64.0 1.5 67.0 1.4 69.0 3.9 74.0 1.7 75.0 2.1 76.0 1.7 77.0 1.3 78.0 8.4 79.0 1.2 80.0 2.1 80.5 4.2 81.0 1.3 82.0 2.1 83.0 1.1 89.0 7.6 90.0 4.8 91.0 1.3 93.0 1.0 104.0 2.2 108.0 2.9 109.0 1.5 116.0 6.1 117.0 16.6 118.0 1.6 121.0 1.1 122.0 1.7 128.0 9.6 129.0 1.5 133.0 1.6 134.0 4.6 135.0 5.7 159.0 1.1 160.0 25.1 161.0 100.0 162.0 11.7 163.0 5.2
400 MHz in CDCl3
90 MHz in CDCl3
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1H NMR 399.65 MHz C9 H7 N S 0.047 g : 0.5 ml CDCl3 2-(2-thienyl)pyridine 
Assign. Shift(ppm)
A 8.559 B 7.65 C 7.64 D 7.565 E 7.382 F 7.12 G 7.098 J(A,F) = 4.6 HZ. J(D,G) = 3.8 HZ. J(D,E) = 1.3 HZ. J(E,G) = 5.1 HZ. J(B,F) = 6.2 HZ. J(C,F) = 2.3 HZ.
Hz ppm Int.3428.22 8.579 33 3424.19 8.568 310 3423.10 8.566 357 3422.61 8.565 374 3421.51 8.562 326 3419.31 8.556 318 3417.97 8.553 478 3416.50 8.549 305 3414.06 8.543 30 3069.46 7.681 35 3067.14 7.675 169 3065.43 7.671 162 3063.84 7.667 57 3063.23 7.665 61 3062.50 7.663 64 3060.91 7.659 97 3059.08 7.655 631 3057.37 7.651 656 3054.57 7.644 665 3053.47 7.641 769 3052.86 7.639 949 3052.12 7.637 864 3051.27 7.635 1000 3046.51 7.623 177 3045.41 7.621 164 3044.19 7.618 71 3042.85 7.614 55 3041.87 7.612 39 3041.14 7.610 37 3026.00 7.572 756 3024.90 7.569 762 3022.34 7.563 765 3021.12 7.560 771 2953.00 7.389 736 2951.78 7.386 706 2949.58 7.381 68 2947.88 7.377 780 2946.78 7.374 774 2854.49 7.143 42 2851.44 7.135 398 2849.12 7.130 351 2847.66 7.126 91 2846.56 7.123 400 2845.21 7.120 386 2843.99 7.117 385 2842.77 7.114 393 2840.94 7.109 944 2840.45 7.108 471 2837.89 7.101 442 2837.28 7.100 899 2835.94 7.097 829 2832.28 7.087 765
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1H NMR 89.56 MHz C9 H7 N S 0.043 g : 0.5 ml CDCl3 2-(2-thienyl)pyridine Assign. Shift(ppm)
A 8.55 B 7.67 C 7.62 D 7.57 E 7.371 F 7.11 G 7.10
Hz ppm Int.769.88 8.597 181 768.38 8.580 253 767.06 8.565 198 765.06 8.543 206 763.69 8.528 328 762.25 8.512 191 687.44 7.676 442 685.81 7.658 761 684.75 7.646 470 682.38 7.620 1000 681.00 7.604 819 679.94 7.593 543 678.75 7.579 560 676.25 7.551 536 675.13 7.539 578 672.88 7.514 69 663.75 7.412 410 662.56 7.398 388 660.31 7.373 79 658.63 7.355 625 657.44 7.341 518 643.19 7.182 273 639.13 7.137 792 638.31 7.128 463 637.19 7.115 124 635.50 7.096 655 634.06 7.080 639 630.38 7.039 450 629.75 7.032 221
in CDCl3
KBr disc
nujol mull
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