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2,2-Bis(bromomethyl)propane-1,3-diol

Product Name 2,2-Bis(bromomethyl)propane-1,3-diol

CAS3296-90-0

MFC5H10Br2O2

MW261.94

¹³CNMR

Mass

MS-NW-8180          
2,2-bis(bromomethyl)-1,3-propanediol
C5H10Br2O2          (Mass of molecular ion:    260)

   Source Temperature: 150 °C
   Sample Temperature: 110 °C
   Direct, 75 eV

      15.0       1.2
      18.0       4.5
      26.0       1.1
      27.0      12.6
      28.0       2.9
      29.0      13.3
      31.0      35.8
      38.0       2.1
      39.0      23.5
      40.0       3.5
      41.0      47.2
      42.0       5.6
      43.0      45.0
      44.0       2.4
      49.0       1.8
      50.0       1.0
      51.0       2.6
      52.0       1.0
      53.0      43.9
      54.0       4.4
      55.0      29.1
      56.0       1.9
      57.0      13.4
      69.0       8.6
      70.0       4.0
      71.0      70.0
      72.0       3.2
      80.0       1.5
      82.0       1.5
      83.0       6.9
      93.0       2.5
      95.0       2.4
     101.0       7.4
     107.0       1.0
     109.0       1.0
     119.0       2.9
     121.0       4.7
     123.0       2.7
     132.0       7.3
     133.0      41.2
     134.0       9.0
     135.0      41.2
     136.0       2.0
     137.0       1.9
     149.0       2.6
     150.0      10.8
     151.0      48.1
     152.0      12.6
     153.0      44.5
     154.0       2.0
     163.0       5.8
     165.0       5.7
     181.0      10.9
     183.0      10.7
     212.0      51.2
     213.0       2.4
     214.0     100.0
     215.0       4.4
     216.0      48.6
     217.0       2.2

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₅ H₁₀ Br₂ O₂	saturated in CDCl₃
2,2-bis(bromomethyl)-1,3-propanediol

    Assign.     Shift(ppm)

      A             3.768
      B             3.521
      C             2.10

     Hz     ppm     Int.

   1505.98   3.769    175
   1407.35   3.522   1000
    840.94   2.105     32

in CDCl3

KBr disc

nujol mull

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