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MS-NW-5617 4-methoxy-3-methylbenzaldehyde C9H10O2 (Mass of molecular ion: 150)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 1.1 27.0 2.3 28.0 1.1 29.0 1.6 38.0 1.7 39.0 5.9 41.0 1.0 50.0 3.8 51.0 8.4 52.0 4.4 53.0 2.5 62.0 1.7 63.0 4.5 64.0 1.1 65.0 5.5 74.0 1.4 75.0 1.0 77.0 15.0 78.0 7.3 79.0 3.7 89.0 2.8 90.0 1.7 91.0 28.2 92.0 2.7 93.0 1.2 105.0 2.5 106.0 5.9 107.0 3.6 119.0 1.3 121.0 7.4 122.0 1.8 135.0 2.4 149.0 100.0 150.0 78.9 151.0 8.0
90 MHz in CDCl3
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1H NMR 89.56 MHz C9 H10 O2 0.04 ml : 0.5 ml CDCl3 4-methoxy-3-methylbenzaldehyde Assign. Shift(ppm)
A 9.849 B 7.71 C 7.67 D 6.920 E 3.908 F 2.254
Hz ppm Int.
882.13 9.850 324 695.80 7.770 28 695.29 7.764 28 693.60 7.745 53 693.16 7.740 53 688.40 7.687 52 687.52 7.677 86 686.65 7.667 180 686.06 7.661 197 623.88 6.967 76 622.12 6.947 24 616.85 6.888 23 614.79 6.865 61 350.02 3.909 1000 201.86 2.254 529
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