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MassMS-NW-9702 5-nitroindoline C8H8N2O2 (Mass of molecular ion: 164)
Source Temperature: 120 °C Sample Temperature: 90 °C Direct, 75 eV
17.0 1.2 18.0 5.9 38.0 1.1 39.0 4.6 41.0 1.2 50.0 1.8 51.0 3.5 52.0 2.3 53.0 1.0 58.5 1.1 62.0 2.7 63.0 8.8 64.0 2.3 65.0 6.6 66.0 1.0 76.0 1.0 77.0 3.2 78.0 2.3 79.0 3.0 89.0 16.8 90.0 15.6 91.0 21.2 92.0 2.6 104.0 1.2 106.0 2.9 116.0 6.9 117.0 48.2 118.0 47.4 119.0 4.3 132.0 1.1 134.0 22.1 135.0 2.2 146.0 2.5 148.0 2.1 163.0 4.5 164.0 100.0 165.0 10.0
400 MHz in CDCl3
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1H NMR 399.65 MHz C8 H8 N2 O2 0.035 g : 0.5 ml CDCl3 5-nitroindoline 
Assign. Shift(ppm)
A 7.972 B 7.914 C 6.468 D 4.73 E 3.761 F 3.104
Hz ppm Int.3191.89 7.987 275 3189.58 7.981 317 3183.11 7.965 279 3180.91 7.960 338 3165.28 7.921 281 3164.06 7.918 497 3162.96 7.915 466 3161.87 7.912 434 2589.36 6.480 640 2584.84 6.468 30 2580.69 6.458 631 1888.92 4.727 104 1512.45 3.785 540 1503.78 3.763 1000 1495.12 3.742 662 1248.54 3.125 362 1240.23 3.104 650 1231.69 3.082 329
in CDCl3
KBr disc
nujol mull
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