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MassMS-NW-9682 (trimethylsilyl)methanol C4H12OSi (Mass of molecular ion: 104)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
29.0 1.4 31.0 1.0 42.0 1.0 43.0 5.9 44.0 1.8 45.0 22.4 46.0 1.5 47.0 2.4 58.0 1.5 59.0 3.0 61.0 43.2 62.0 2.8 63.0 1.6 72.0 4.5 73.0 100.0 74.0 9.7 75.0 6.0 89.0 7.5 104.0 3.9
400 MHz in CDCl3
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1H NMR 399.65 MHz C4 H12 O Si 0.05 ml : 0.5 ml CDCl3 (trimethylsilyl)methanol 
Assign. Shift(ppm)
A 3.348 B 2.42 C 0.060 J(SI-29,H(C))=6.7HZ J(C-13,H(C))=119HZ
Hz ppm Int.1338.26 3.349 632 968.02 2.423 152 82.40 0.207 31 26.86 0.068 442 23.93 0.060 1000 20.02 0.051 300 -36.73 -0.091 27
in CDCl3
liquid film
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