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MassMS-NW-6602 2-fluorobiphenyl C12H9F (Mass of molecular ion: 172)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
39.0 1.6 50.0 2.4 51.0 3.0 57.0 1.0 62.0 1.2 63.0 2.8 73.0 3.2 74.0 2.4 75.0 3.3 76.0 3.1 85.0 6.2 85.5 1.1 86.0 4.0 94.0 1.4 99.0 1.3 107.0 1.0 120.0 2.9 125.0 1.7 126.0 1.1 133.0 4.1 144.0 1.8 145.0 1.2 146.0 4.9 150.0 1.8 151.0 3.8 152.0 4.8 153.0 1.6 157.0 1.5 168.0 1.0 169.0 3.4 170.0 18.4 171.0 27.7 172.0 100.0 173.0 12.8
400 MHz in CDCl3
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1H NMR 399.65 MHz C12 H9 F 0.051 g : 0.5 ml CDCl3 2-fluorobiphenyl 
Assign. Shift(ppm)
A 7.543 B 7.45 to 7.40 C 7.355 D 7.286 E 7.186 G 7.135
Hz ppm Int.3026.49 7.573 30 3024.41 7.568 34 3020.87 7.559 297 3019.29 7.555 584 3017.70 7.551 449 3015.63 7.546 150 3014.16 7.543 186 3013.55 7.541 221 3012.45 7.538 528 3011.84 7.537 446 3010.99 7.535 588 3009.40 7.531 383 3007.45 7.526 73 2981.81 7.462 35 2979.98 7.457 48 2978.03 7.452 169 2977.29 7.450 319 2976.32 7.448 521 2975.22 7.445 264 2974.85 7.444 281 2973.39 7.440 254 2971.07 7.435 217 2970.70 7.434 230 2969.12 7.430 1000 2967.65 7.426 734 2965.45 7.421 428 2962.89 7.414 309 2961.55 7.411 476 2960.82 7.409 415 2959.72 7.406 308 2957.89 7.402 263 2948.85 7.379 31 2946.53 7.373 236 2945.07 7.370 445 2943.73 7.366 246 2941.65 7.361 35 2939.94 7.357 169 2937.74 7.351 400 2935.42 7.345 133 2931.76 7.336 113 2930.42 7.333 187 2929.08 7.330 103 2924.19 7.317 112 2922.36 7.313 107 2919.19 7.305 116 2916.75 7.299 181 2916.02 7.297 160 2914.92 7.294 156 2914.18 7.292 155 2911.74 7.286 180 2911.01 7.284 153 2909.91 7.282 168 2908.57 7.278 217 2906.74 7.274 184 2903.69 7.266 190 2901.73 7.261 175 2879.15 7.205 323 2877.81 7.201 378 2873.78 7.191 37 2871.70 7.186 448 2870.36 7.183 516 2867.80 7.176 30 2866.33 7.173 33 2864.14 7.167 222 2862.92 7.164 232 2861.21 7.160 276 2859.86 7.156 231 2853.03 7.139 206 2851.81 7.136 202 2850.46 7.133 275 2849.12 7.130 256 2842.29 7.112 194 2840.94 7.109 187
in CDCl3
KBr disc
nujol mull
4880 A,200 M,powder
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