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321-38-0

1-Fluoronaphthalene

Product Name 1-Fluoronaphthalene

CAS321-38-0

MFC10H7F

MW146.16

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  • 321-38-0_ms
    Mass 

    MS-NW-5447          
1-fluoronaphthalene
C10H7F              (Mass of molecular ion:    146)


       Source Temperature: 260 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV


          50.0       2.3
      51.0       1.7
      60.0       2.5
      62.0       1.3
      63.0       2.2
      72.0       1.3
      73.0       5.7
      74.0       2.8
      75.0       3.5
      94.0       1.7
      96.0       1.8
      98.0       1.1
      99.0       2.4
     120.0       6.1
     125.0       5.6
     126.0       3.8
     127.0       1.0
     144.0       3.2
     145.0       7.2
     146.0     100.0
     147.0      11.1

90 MHz in CDCl3

400 MHz in CDCl3

  • 321-38-0_1hnmr

    1H NMR 89.56 MHz
    C10 H7 F 0.04 ml : 0.5 ml CDCl3
    1-fluoronaphthalene
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             8.08
      B             7.80
      C             7.55
      D     *1      7.50
      E     *1      7.48
      G             7.31
      J             7.11
  

         Hz     ppm     Int.


        729.50   8.146    130
    726.75   8.115    126
    726.13   8.108    151
    724.56   8.091    101
    723.88   8.083    100
    723.19   8.075     69
    722.44   8.067     94
    721.50   8.057     73
    719.88   8.038    187
    706.13   7.885     67
    705.75   7.881     70
    705.38   7.877     70
    705.00   7.872     66
    704.00   7.861     76
    703.19   7.852     98
    701.63   7.835    107
    699.50   7.811    167
    697.50   7.789    136
    696.19   7.774    133
    695.81   7.770    127
    694.38   7.754    137
    692.44   7.732     57
    684.31   7.641    115
    683.88   7.637    130
    683.44   7.632    155
    682.44   7.620    128
    678.88   7.581    101
    678.00   7.571     99
    676.19   7.551    276
    674.88   7.536   1000
    672.06   7.505    302
    671.25   7.495    395
    668.88   7.469    319
    668.06   7.460    410
    666.56   7.443     48
    665.31   7.429    612
    662.56   7.398    229
    660.44   7.375    353
    655.06   7.315    305
    652.38   7.285    197
    646.94   7.224    192
    645.50   7.208    251
    643.94   7.191    242
    638.06   7.125    120
    636.44   7.107    104
    634.88   7.089    235
    633.56   7.075    235
    627.38   7.006    129
    626.06   6.991    122

  • 321-38-0_1hnmr_2

    1H NMR 399.65 MHz
    C10 H7 F 0.05 ml : 0.5 ml CDCl3
    1-fluoronaphthalene
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             8.09
      B             7.80
      C             7.564
      D     *1      7.49
      E     *1      7.47
      G             7.331
      J             7.103
     
     J(F-19,G) = 5.4 HZ.
     J(F-19,J) = 10.7 HZ.
     J(G,J)= 7.7 HZ.
     J(C,J)= 1.0 HZ.
     J(C,G) = 8.3 HZ.
  

         Hz     ppm     Int.


       3242.68   8.114     31
   3240.36   8.108     71
   3237.30   8.101    347
   3235.11   8.095    240
   3233.03   8.090    305
   3227.66   8.077    403
   3124.39   7.818     66
   3121.95   7.812    230
   3120.24   7.808    344
   3118.65   7.804    209
   3116.70   7.799    255
   3115.11   7.795    293
   3112.92   7.790    355
   3110.72   7.784    275
   3107.18   7.775     72
   3027.59   7.576    567
   3019.29   7.555    678
   3010.38   7.533     30
   3006.59   7.524     41
   3004.52   7.518     40
   3000.98   7.510     98
   2998.90   7.504    192
   2994.14   7.492    626
   2992.55   7.488    870
   2988.53   7.478   1000
   2984.50   7.468    715
   2983.03   7.465    677
   2978.27   7.453    188
   2976.20   7.448    100
   2973.39   7.440     33
   2973.02   7.440     33
   2972.17   7.437     34
   2940.31   7.358    325
   2934.94   7.344    339
   2932.50   7.338    463
   2927.12   7.325    461
   2924.44   7.318    342
   2918.95   7.304    318
   2848.02   7.127    369
   2847.05   7.124    403
   2840.33   7.108    335
   2839.36   7.105    363
   2837.28   7.100    396
   2836.30   7.097    414
   2829.59   7.081    317
   2828.74   7.079    344

in CDCl3

  • 321-38-0_13cnmr

liquid film

  • 321-38-0_ir1

  • 321-38-0_raman

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