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317-17-9

Pyrrolo[1,2-a]quinoline

Product Name Pyrrolo[1,2-a]quinoline

CAS317-17-9

MFC12H9N

MW167.21

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parameter in CDCl3

parameter in DMSO-d6

  • 317-17-9_1hnmr_2

    1H NMR 300 MHz
    C12 H9 N 5 wt% in CDCl3
    pyrrolo(1,2-a)quinoline
    ChemicalStructure
        Parameter     ppm  Hz
    D(A) 7.79 D(B) 6.76 D(C) 6.50 D(D) 7.269 D(E) 6.935 D(F) 7.586 D(G) 7.265 D(J) 7.442 D(K) 7.825 J(A,B) 2.9 J(A,C) 1.4 J(A,D) 0.7 J(A,E) 0.25 J(A,F) 0.0 J(A,G) 0.0 J(A,J) 0.0 J(A,K) 0.2 J(B,C) 3.8 J(B,D) 0.0 J(B,E) 0.0 J(B,F) 0.0 J(B,G) 0.0 J(B,J) 0.0 J(B,K) 0.0 J(C,D) -0.28 J(C,E) 0.28 J(C,F) 0.0 J(C,G) 0.0 J(C,J) 0.0 J(C,K) 0.0 J(D,E) 9.35 J(D,F) 0.34 J(D,G) 0.0 J(D,J) 0.29 J(D,K) 0.0 J(E,F) -0.37 J(E,G) 0.0 J(E,J) 0.0 J(E,K) 0.74 J(F,G) 7.83 J(F,J) 1.50 J(F,K) 0.54 J(G,J) 7.27 J(G,K) 1.11 J(J,K) 8.38 HEFFERNAN,M.L. & IRVINE,G.M. AUST.J.CHEM. 29, 837 (1976) J(A,B).J(A,C) AND J(B,C) : FROM SPECTRUM AT -20 C. J(A,D),J(A,E),J(A,K),J(C,D),J(C,E) : IN DMSO-D6

         Hz     ppm     Int.
    

       2351.82   7.839    489
       2343.47   7.812    574
       2338.79   7.796    477
       2338.10   7.794    490
       2337.45   7.791    485
       2336.57   7.789    487
       2335.92   7.786    496
       2335.27   7.784    479
       2280.53   7.602    403
       2279.20   7.597    422
       2272.76   7.576    472
       2271.42   7.571    501
       2241.25   7.471    287
       2239.74   7.466    279
       2233.96   7.447    411
       2232.63   7.442    497
       2231.46   7.438    285
       2225.64   7.419    332
       2224.13   7.414    303
       2187.16   7.291    514
       2185.97   7.287   1000
       2179.41   7.265    569
       2178.75   7.262    560
       2178.35   7.261    546
       2176.28   7.254    819
       2172.13   7.240    299
       2171.01   7.237    288
       2084.99   6.950    768
       2075.61   6.919    637
       2031.38   6.771    629
       2028.47   6.762    716
       2027.61   6.759    779
       2024.70   6.749    679
       1952.53   6.508    603
       1951.17   6.504    615
       1948.75   6.496    565
       1947.38   6.491    549
    

  • 317-17-9_1hnmr_0

    1H NMR 300 MHz
    C12 H9 N 5 wt% in DMSO-d6
    pyrrolo(1,2-a)quinoline
    ChemicalStructure
        Parameter     ppm  Hz
    D(A) 8.215 D(B) 6.773 D(C) 6.541 D(D) 7.400 D(E) 7.087 D(F) 7.748 D(G) 7.365 D(J) 7.558 D(K) 8.208 J(A,B) 2.89 J(A,C) 1.44 J(A,D) 0.66 J(A,E) 0.25 J(A,F) 0.0 J(A,G) 0.0 J(A,J) 0.0 J(A,K) 0.25 J(B,C) 3.77 J(B,D) 0.0 J(B,E) 0.0 J(B,F) 0.0 J(B,G) 0.0 J(B,J) 0.0 J(B,K) 0.0 J(C,D) -0.28 J(C,E) 0.28 J(C,F) 0.0 J(C,G) 0.0 J(C,J) 0.0 J(C,K) 0.0 J(D,E) 9.33 J(D,F) 0.33 J(D,G) 0.30 J(D,J) 0.0 J(D,K) 0.0 J(E,F) -0.33 J(E,G) 0.0 J(E,J) 0.0 J(E,K) 0.62 J(F,G) 7.87 J(F,J) 1.52 J(F,K) 0.51 J(G,J) 7.24 J(G,K) 1.08 J(J,K) 8.42 HEFFERNAN,M.L. & IRVINE,G.M. AUST.J.CHEM 29, 837 (1976)

         Hz     ppm     Int.
    

       2466.52   8.222    956
       2464.08   8.214    553
       2462.72   8.209    502
       2458.32   8.194    568
       2329.17   7.764    402
       2327.77   7.759    421
       2321.29   7.738    463
       2319.96   7.733    484
       2276.13   7.587    263
       2274.58   7.582    259
       2268.85   7.563    379
       2267.47   7.558    490
       2266.24   7.554    289
       2260.48   7.535    313
       2258.95   7.530    297
       2224.89   7.416    640
       2215.88   7.386   1000
       2209.17   7.364    538
       2202.09   7.340    242
       2201.14   7.337    238
       2130.54   7.102    793
       2121.21   7.071    647
       2035.28   6.784    506
       2032.32   6.774    637
       2031.56   6.772    687
       2028.64   6.762    563
       1964.81   6.549    543
       1963.45   6.545    558
       1961.06   6.537    518
       1959.68   6.532    496
    

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