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MassMS-NW-6343 2-amino-9-fluorenone C13H9NO (Mass of molecular ion: 195)
Source Temperature: 190 °C Sample Temperature: 140 °C Direct, 75 eV
39.0 1.1 62.0 1.3 63.0 2.3 69.5 2.5 70.0 1.3 70.5 2.4 74.0 1.2 75.0 1.2 82.5 1.7 83.5 6.1 86.0 1.0 87.0 1.4 89.0 1.3 97.5 2.8 113.0 1.7 114.0 1.1 115.0 1.1 138.0 1.5 139.0 14.6 140.0 6.3 141.0 1.1 150.0 1.1 164.0 1.1 166.0 5.2 167.0 6.1 168.0 3.2 194.0 2.3 195.0 100.0 196.0 14.7 197.0 1.3
400 MHz in CDCl3
90 MHz in CDCl3
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1H NMR 399.65 MHz C13 H9 N O saturated in CDCl3 2-amino-9-fluorenone 
Assign. Shift(ppm)
A 7.549 B 7.382 C 7.320 D 7.252 E 7.133 F 6.957 G 6.709 J 3.91 J(A,B) = 1.2 HZ, J(A,E) = 7.3 HZ, J(B,C) = 7.5 HZ, J(C,E) = 1.0 HZ, J(D,G) = 7.9 HZ, J(F,G) = 2.2 HZ.
Hz ppm Int.3021.61 7.561 406 3020.87 7.559 570 3020.02 7.557 435 3014.28 7.543 443 3013.55 7.541 619 2959.35 7.405 243 2958.13 7.402 254 2956.18 7.397 43 2951.90 7.387 643 2950.68 7.384 655 2947.75 7.376 48 2947.39 7.375 47 2944.46 7.368 487 2943.24 7.365 478 2935.18 7.345 35 2933.72 7.341 32 2928.71 7.329 544 2927.98 7.327 824 2924.07 7.317 57 2923.46 7.316 55 2921.26 7.310 348 2920.53 7.308 488 2902.22 7.262 985 2898.19 7.252 61 2897.83 7.251 61 2894.29 7.243 961 2890.50 7.233 36 2860.47 7.158 36 2857.79 7.151 398 2856.81 7.149 393 2854.13 7.142 48 2850.46 7.133 682 2849.37 7.130 679 2843.02 7.114 320 2842.04 7.112 313 2781.49 6.960 943 2779.30 6.955 1000 2686.16 6.722 677 2683.84 6.716 651 2678.22 6.702 634 2675.90 6.696 608 1562.74 3.911 138
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1H NMR 89.56 MHz C13 H9 N O 0.049 g : 0.5 ml CDCl3 2-amino-9-fluorenone Assign. Shift(ppm)
A 7.54 B 7.38 C 7.32 D 7.25 E 7.13 F 6.95 G 6.70 J 3.89 B,C AND E WERE CONFIRMED BY LAOCN PROGRAM. 400MHZ : HSP-41-745
Hz ppm Int.679.75 7.590 310 676.76 7.557 111 676.33 7.552 107 672.49 7.509 452 667.36 7.452 95 666.33 7.441 90 662.92 7.402 281 661.72 7.389 291 655.74 7.322 1000 653.52 7.298 625 650.78 7.267 369 650.27 7.261 361 645.14 7.204 795 638.56 7.130 264 637.96 7.124 271 636.34 7.106 234 633.09 7.069 103 631.73 7.054 134 630.62 7.042 107 629.76 7.032 115 629.33 7.027 121 623.69 6.964 515 621.73 6.943 595 604.81 6.754 365 602.50 6.728 319 596.86 6.665 271 594.73 6.641 240 347.61 3.882 339
in CDCl3
KBr disc
nujol mull
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