-
MassMS-IW-5465 cyclohexyl acrylate C9H14O2 (Mass of molecular ion: 154)
Source Temperature: 230 °C Sample Temperature: 150 °C Reservoir, 75 eV
26.0 3.1 27.0 16.3 28.0 2.5 29.0 3.6 39.0 8.1 40.0 1.2 41.0 15.9 42.0 2.1 43.0 2.5 44.0 1.5 51.0 1.2 53.0 3.7 54.0 26.2 55.0 100.0 56.0 5.2 57.0 2.5 66.0 1.0 67.0 66.1 68.0 4.3 69.0 1.0 70.0 7.3 71.0 1.3 72.0 3.0 73.0 26.5 74.0 1.1 77.0 1.3 79.0 2.8 80.0 1.0 81.0 9.8 82.0 89.8 83.0 13.4 84.0 1.7 94.0 3.2 95.0 1.3 97.0 1.1 98.0 1.9 99.0 5.6 111.0 1.2
400 MHz in CDCl3
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1H NMR 399.65 MHz C9 H14 O2 0.05 ml : 0.5 ml CDCl3 cyclohexyl acrylate 
Assign. Shift(ppm)
A 6.378 B 6.108 C 5.789 D 4.836 E 1.88 F 1.74 G 1.55 J 1.45 K 1.39 L 1.281 J(A,B)=17.3HZ J(A,C)=1.6HZ J(B,C)=10.4HZ
Hz ppm Int.2559.94 6.406 740 2558.35 6.402 745 2542.60 6.363 982 2541.02 6.359 975 2454.35 6.142 876 2443.97 6.116 1000 2437.01 6.098 658 2426.64 6.072 760 2319.46 5.804 929 2317.87 5.800 892 2309.08 5.778 784 2307.37 5.774 797 1945.80 4.869 92 1942.14 4.860 208 1938.23 4.850 194 1936.89 4.847 191 1933.11 4.838 374 1929.20 4.828 269 1924.07 4.815 187 1920.17 4.805 114 763.18 1.910 137 759.16 1.900 258 756.10 1.892 293 753.78 1.887 255 750.85 1.879 337 748.54 1.873 286 746.83 1.869 334 745.61 1.866 334 744.63 1.864 327 742.55 1.859 363 708.13 1.772 184 704.71 1.764 237 702.88 1.759 291 702.15 1.757 290 698.97 1.749 313 696.29 1.743 259 693.60 1.736 328 692.63 1.734 334 690.19 1.727 318 687.26 1.720 262 635.13 1.590 48 632.57 1.583 106 631.35 1.580 98 630.25 1.578 118 629.15 1.575 122 628.17 1.572 140 627.32 1.570 170 623.78 1.561 161 620.73 1.554 155 617.92 1.547 175 614.87 1.539 196 612.43 1.533 135 611.45 1.530 151 606.08 1.517 67 604.86 1.514 63 602.54 1.508 167 599.12 1.500 139 592.04 1.482 296 589.11 1.475 340 582.64 1.458 266 579.83 1.451 448 577.39 1.445 283 570.19 1.427 579 567.75 1.421 343 562.50 1.408 241 559.81 1.401 484 556.88 1.394 342 552.61 1.383 151 549.80 1.376 322 546.75 1.369 412 543.95 1.362 201 539.79 1.351 133 536.50 1.343 215 533.57 1.336 136 528.44 1.323 104 525.39 1.315 153 522.46 1.308 99 518.55 1.298 107 516.11 1.292 178 513.43 1.285 178 509.89 1.276 111 506.47 1.268 139 503.05 1.259 159 499.76 1.251 90 496.46 1.243 57 492.92 1.234 61 489.87 1.226 34
in CDCl3
liquid film
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