SPERMINE TETRAHYDROCHLORIDE

Mass

MS-IW-3653          
N,N'-bis(3-aminopropyl)tetramethylenediamine tetrahydrochloride
C10H26N4 4HCl       (Mass of molecular ion:    202)

   Source Temperature: 160 °C
   Sample Temperature: 180 °C
   Direct, 75 eV

      17.0       1.0
      18.0       6.4
      27.0       2.1
      28.0      12.0
      29.0       5.3
      30.0      49.2
      31.0       1.9
      35.0      14.5
      36.0      83.9
      37.0       5.0
      38.0      38.7
      39.0       2.2
      41.0      13.0
      42.0      17.7
      43.0      14.0
      44.0      86.5
      45.0       8.7
      46.0       2.6
      53.0       1.0
      54.0       2.3
      55.0      11.8
      56.0      23.7
      57.0      88.4
      58.0      30.4
      59.0       3.5
      60.0       4.4
      68.0       6.0
      69.0       2.7
      70.0      50.9
      71.0       9.6
      72.0      32.7
      73.0       4.4
      74.0      12.9
      75.0       2.9
      82.0       4.9
      83.0       3.7
      84.0     100.0
      85.0      13.2
      86.0      12.3
      87.0      26.2
      88.0       1.6
      89.0      14.4
      96.0       2.5
      97.0       1.2
      98.0      27.0
      99.0      11.7
     100.0       4.2
     101.0       3.7
     102.0      11.0
     103.0       3.5
     110.0       3.4
     111.0       1.5
     112.0       6.9
     113.0      20.1
     114.0       2.1
     115.0       8.4
     116.0       4.9
     125.0       1.3
     126.0       1.0
     127.0      36.1
     128.0       3.6
     129.0      11.1
     130.0      13.3
     131.0       1.1
     145.0       1.1
     146.0       1.5
     158.0      25.8
     159.0       9.3
     172.0       5.9
     202.0       7.5
     203.0       1.2

Assign. Shift(ppm) A 3.18 B 3.12 C 2.108 D 1.800

     Hz     ppm     Int.

   1277.59   3.197    563
   1269.65   3.177    625
   1261.60   3.157    750
   1254.27   3.139   1000
   1246.46   3.119    982
   1238.65   3.100    696
    858.03   2.147    175
    852.29   2.133    214
    850.10   2.128    342
    848.39   2.123    242
    845.21   2.115    232
    842.29   2.108    585
    839.23   2.100    234
    836.55   2.094    227
    834.23   2.088    315
    832.64   2.084    228
    826.54   2.069    166
    727.42   1.821    246
    723.75   1.811    336
    719.97   1.802    557
    716.19   1.793    349
    712.65   1.784    259