Cholesteryl oleate

Mass

MS-NW-9604          
5-cholesten-3beta-yl oleate
C45H78O2            (Mass of molecular ion:    650)

   Source Temperature: 250 °C
   Sample Temperature: 180 °C
   Direct, 75 eV

      18.0       2.6
      27.0       1.6
      28.0       1.1
      29.0       4.5
      39.0       2.0
      41.0      15.3
      42.0       2.2
      43.0      15.5
      53.0       2.0
      54.0       4.4
      55.0      26.7
      56.0       7.0
      57.0      16.7
      60.0       2.5
      65.0       1.2
      67.0      16.3
      68.0       6.3
      69.0      24.5
      70.0       7.7
      71.0      10.4
      73.0       4.1
      77.0       2.9
      78.0       1.2
      79.0       9.8
      80.0       2.8
      81.0      31.3
      82.0      10.1
      83.0      20.8
      84.0       8.3
      85.0       4.8
      87.0       1.6
      91.0      11.8
      92.0       3.2
      93.0      13.2
      94.0       4.8
      95.0      22.0
      96.0       9.5
      97.0      16.8
      98.0       8.1
      99.0       2.1
     100.0       1.1
     101.0       1.9
     104.0       1.2
     105.0      16.1
     106.0       6.3
     107.0      15.6
     108.0       7.3
     109.0      15.0
     110.0       6.3
     111.0       9.7
     112.0       3.4
     113.0       1.6
     114.0       2.2
     115.0       2.9
     116.0       1.2
     117.0       6.0
     118.0       3.7
     119.0       9.5
     120.0       8.9
     121.0      15.5
     122.0       4.8
     123.0       8.4
     124.0       3.9
     125.0       4.7
     126.0       1.7
     127.0       2.3
     128.0       2.6
     129.0       5.6
     130.0       2.2
     131.0      10.0
     132.0       2.7
     133.0      12.2
     134.0       4.9
     135.0      12.5
     136.0       3.2
     137.0       5.5
     138.0       2.8
     139.0       2.6
     140.0       1.0
     141.0       2.8
     142.0       2.3
     143.0       8.6
     144.0       4.0
     145.0      25.6
     146.0      10.2
     147.0      28.9
     148.0       9.6
     149.0       9.5
     150.0       1.9
     151.0       4.4
     152.0       2.3
     153.0       1.9
     155.0       1.6
     156.0       1.1
     157.0       5.5
     158.0       4.3
     159.0      12.3
     160.0      12.3
     161.0      12.3
     162.0       4.0
     163.0       9.2
     164.0       1.7
     165.0       3.6
     166.0       1.7
     167.0       1.2
     169.0       1.3
     171.0       3.6
     172.0       1.9
     173.0       5.1
     174.0       2.6
     175.0       4.0
     176.0       1.4
     177.0       2.9
     179.0       2.1
     180.0       1.6
     181.0       1.1
     183.0       1.2
     185.0       4.4
     186.0       1.6
     187.0       2.3
     189.0       1.7
     191.0       3.1
     192.0       1.1
     193.0       3.2
     194.0       1.4
     197.0       2.9
     198.0       1.1
     199.0       4.4
     200.0       2.9
     201.0       4.4
     202.0       1.1
     203.0       1.2
     205.0       2.8
     206.0       3.7
     207.0       2.4
     208.0       1.0
     211.0       1.8
     212.0       1.1
     213.0      12.1
     214.0       3.8
     215.0       3.5
     216.0       1.3
     217.0       1.1
     219.0       2.2
     220.0       1.9
     221.0       1.4
     222.0       1.5
     227.0       2.2
     228.0       3.6
     229.0       3.4
     230.0       1.0
     231.0       1.2
     235.0       1.1
     239.0       1.0
     241.0       1.6
     243.0       1.0
     245.0       2.6
     246.0       5.0
     247.0      26.1
     248.0       5.6
     253.0       2.1
     254.0       1.1
     255.0      19.8
     256.0       5.0
     257.0       2.6
     258.0       1.2
     259.0       2.6
     260.0      19.9
     261.0       5.8
     262.0       1.1
     264.0       5.4
     265.0       1.4
     274.0       2.4
     275.0       1.3
     282.0       1.4
     283.0       2.2
     284.0       1.1
     314.0       1.5
     326.0       2.9
     327.0       1.0
     351.0       1.1
     352.0       1.2
     353.0      20.0
     354.0       5.8
     355.0       2.2
     366.0       3.7
     367.0       2.4
     368.0     100.0
     369.0      36.8
     370.0       8.6
     371.0       1.5

Assign. Shift(ppm) A 5.38 B 5.34 C 4.617 D 2.31 E 2.264 F 1.30 to 1.27 L 1.018 M 0.915 N 0.88 P *1 0.867 Q *1 0.862 R 0.676

     Hz     ppm     Int.

   2149.29   5.378    145
   2146.48   5.371    115
   2146.12   5.370    115
   2144.65   5.367    110
   2144.29   5.366    111
   2141.60   5.359     97
   2138.79   5.352     75
   2137.82   5.350     75
   2135.74   5.345    154
   2133.18   5.338     65
   2132.20   5.336     68
   2129.64   5.329     61
   1848.63   4.626     43
   1838.99   4.602     45
    926.88   2.320    154
    919.56   2.301    124
    912.23   2.283    155
    904.79   2.264    245
    897.22   2.246    149
    800.17   2.003    200
    735.96   1.842    147
    599.85   1.501    159
    538.33   1.348    233
    535.89   1.341    254
    530.88   1.329    372
    530.64   1.328    372
    529.79   1.326    371
    520.51   1.303    673
    506.35   1.267    673
    501.83   1.256    532
    450.93   1.129    210
    407.23   1.019   1000
    402.71   1.008    151
    393.55   0.985    114
    382.32   0.957    113
    376.83   0.943     94
    376.46   0.942     94
    368.90   0.924    498
    366.09   0.917    150
    362.43   0.907    484
    358.64   0.898    230
    355.83   0.891    166
    352.05   0.881    543
    349.73   0.876    927
    347.90   0.871    914
    344.73   0.863    315
    343.14   0.859    850
    341.31   0.855    819
    270.51   0.677    971