grayanotoxin IV(30272-17-4) IR Spectrum

Mass

MS2001-00304WA      
(3beta,6beta,14R)-10(20)-grayanotoxene-3,5,6,14,16-pentol 14-acetate
C22H34O6            (Mass of molecular ion:    394)

   Source Temperature: 205 °C
   Sample Temperature:  45 °C
   Direct, 70 eV

      15.0       1.2
      18.0       4.1
      27.0       2.1
      29.0       4.0
      31.0       1.1
      39.0       2.8
      41.0      17.4
      42.0       1.9
      43.0     100.0
      44.0       3.0
      45.0       2.4
      53.0       5.6
      54.0       1.0
      55.0      13.8
      56.0       1.3
      57.0       6.6
      58.0       3.2
      59.0       2.2
      61.0       3.6
      65.0       3.2
      66.0       1.5
      67.0      11.2
      68.0       1.3
      69.0      23.3
      70.0       2.4
      71.0       9.4
      72.0       3.5
      73.0       1.1
      77.0       9.7
      78.0       2.6
      79.0      15.2
      80.0       3.6
      81.0      11.8
      82.0       3.3
      83.0       6.7
      84.0       1.2
      85.0       2.7
      87.0       1.0
      91.0      22.9
      92.0       5.9
      93.0      20.3
      94.0       5.5
      95.0      11.5
      96.0       2.7
      97.0       3.0
      99.0       1.4
     101.0       2.5
     103.0       2.8
     104.0       2.2
     105.0      20.1
     106.0       6.5
     107.0      16.9
     108.0       6.1
     109.0      21.0
     110.0       3.5
     111.0       4.1
     112.0       1.1
     113.0       1.1
     115.0       4.8
     116.0       2.9
     117.0      11.6
     118.0       4.6
     119.0      17.7
     120.0       7.5
     121.0      12.1
     122.0       5.0
     123.0       5.5
     124.0       2.0
     125.0       1.9
     127.0       1.7
     128.0       5.2
     129.0      10.8
     130.0       6.1
     131.0      17.6
     132.0       6.6
     133.0      17.2
     134.0       9.5
     135.0      20.7
     136.0       8.1
     137.0       6.6
     138.0       2.5
     139.0       2.1
     141.0       4.9
     142.0       5.0
     143.0      14.2
     144.0       7.7
     145.0      20.4
     146.0       7.5
     147.0      12.7
     148.0      14.4
     149.0       8.4
     150.0       5.2
     151.0       4.2
     152.0       2.1
     153.0       2.7
     154.0       1.8
     155.0       6.4
     156.0       4.4
     157.0      12.5
     158.0       7.7
     159.0      18.0
     160.0       7.9
     161.0      12.7
     162.0       6.6
     163.0      12.9
     164.0       4.3
     165.0       3.8
     166.0       5.3
     167.0       4.9
     168.0       2.8
     169.0      12.1
     170.0       5.6
     171.0      14.6
     172.0       8.6
     173.0      13.8
     174.0       6.6
     175.0       7.9
     176.0       5.3
     177.0       4.9
     178.0       2.4
     179.0       6.3
     180.0       3.4
     181.0       5.3
     182.0       3.4
     183.0      10.5
     184.0       7.4
     185.0      12.2
     186.0       6.9
     187.0      16.6
     188.0      11.3
     189.0      11.5
     190.0       5.2
     191.0       3.9
     192.0       2.3
     193.0       2.5
     194.0       2.6
     195.0       4.5
     196.0       2.8
     197.0      12.7
     198.0       5.3
     199.0       9.2
     200.0       5.1
     201.0      15.3
     202.0      10.1
     203.0       6.5
     204.0       3.6
     205.0       4.4
     206.0      10.6
     207.0       5.1
     208.0       1.8
     209.0       8.2
     210.0       3.1
     211.0      10.9
     212.0      13.9
     213.0      12.0
     214.0       7.2
     215.0      12.3
     216.0       4.3
     217.0       4.2
     218.0       1.8
     219.0       3.9
     220.0       2.2
     221.0       2.0
     222.0       2.7
     223.0       4.2
     224.0       3.0
     225.0       8.4
     226.0       6.6
     227.0      16.8
     228.0       6.4
     229.0      14.7
     230.0      15.0
     231.0       5.6
     232.0       2.1
     233.0       2.6
     234.0       1.5
     235.0       1.1
     237.0       9.4
     238.0       3.9
     239.0       4.8
     240.0      10.4
     241.0      14.5
     242.0       6.1
     243.0       4.6
     244.0       3.0
     245.0       7.2
     246.0       2.3
     247.0       7.1
     248.0       4.0
     249.0       1.3
     251.0       3.5
     252.0       8.4
     253.0       4.2
     254.0       5.1
     255.0      24.3
     256.0       8.2
     257.0       4.0
     258.0      12.7
     259.0       6.3
     260.0       2.3
     261.0       1.9
     262.0       1.2
     263.0       1.0
     265.0       4.1
     266.0       1.1
     267.0       1.7
     269.0      10.7
     270.0      18.0
     271.0       6.8
     272.0       4.7
     273.0      16.5
     274.0       3.9
     275.0       1.0
     276.0       4.5
     277.0       1.1
     279.0       1.2
     280.0      13.1
     281.0       4.2
     282.0       1.0
     283.0       6.6
     284.0       1.5
     285.0       1.7
     287.0       3.8
     288.0       4.9
     289.0       2.6
     290.0       2.4
     291.0       1.7
     297.0       1.7
     298.0      40.7
     299.0      10.4
     300.0       2.0
     301.0       3.9
     302.0       1.0
     315.0       2.6
     316.0      24.7
     317.0       7.4
     318.0       1.5
     333.0       1.1
     334.0       1.9
     340.0       1.8
     348.0       9.8
     349.0       2.3
     358.0      10.3
     359.0       2.6
     376.0       7.1
     377.0       1.8
     394.0       1.0

KBr disc

nujol mull