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Dimethoxymethylphenylsilane

Product Name Dimethoxymethylphenylsilane

CAS3027-21-2

MFC9H14O2Si

MW182.29

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  • Mass 

    MS-IW-7190          
dimethoxymethylphenylsilane
C9H14O2Si           (Mass of molecular ion:    182)


       Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV


          43.0       1.6
      45.0       2.7
      51.0       1.5
      59.0       9.6
      74.0       1.3
      75.0       6.8
      77.0       1.5
      78.0       1.1
      83.5       1.5
      91.0      15.4
      92.0       1.4
     104.0       1.0
     105.0       7.4
     107.0       7.8
     121.0       5.0
     137.0      28.4
     138.0       3.7
     139.0       1.2
     151.0       3.6
     167.0     100.0
     168.0      14.0
     169.0       4.6
     182.0      11.9
     183.0       1.8

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C9 H14 O2 Si 0.05 ml : 0.5 ml CDCl3
    dimethoxymethylphenylsilane
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             7.619
      B             7.41
      C             7.37
      D             3.555
      E             0.350
     
     CONFIRMED BY LAOCN PROGRAM
  

         Hz     ppm     Int.


       3049.32   7.630    120
   3047.73   7.626    139
   3046.39   7.623     69
   3045.78   7.622     54
   3043.70   7.616     51
   3042.60   7.614     55
   3041.75   7.612    128
   3039.79   7.607    136
   2962.40   7.413     57
   2961.91   7.412     64
   2959.11   7.405     37
   2957.28   7.400     74
   2955.44   7.396    122
   2953.61   7.391    152
   2953.13   7.390    137
   2952.39   7.388     90
   2951.54   7.386     80
   2948.36   7.378     55
   2947.39   7.375     74
   2946.66   7.374     75
   2946.04   7.372    121
   2945.43   7.371     98
   2944.46   7.368     41
   2939.82   7.356     49
   2937.26   7.350     31
   1422.73   3.560    192
   1420.78   3.556   1000
   1418.70   3.550    170
    143.55   0.360     55
    140.01   0.351    719
    136.35   0.342     50

in CDCl3



liquid film



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