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Didodecylamine

Product Name Didodecylamine

CAS3007-31-6

MFC24H51N

MW353.67

¹³CNMR

Mass

MS-IW-3877          
didodecylamine
C24H51N             (Mass of molecular ion:    353)

   Source Temperature: 150 °C
   Sample Temperature: 130 °C
   Direct, 75 eV

      18.0       1.6
      29.0       2.4
      30.0       9.5
      41.0       5.3
      42.0       1.6
      43.0      11.5
      44.0      24.0
      45.0       1.1
      55.0       6.0
      56.0       3.8
      57.0       7.4
      58.0       1.8
      69.0       3.2
      70.0       3.2
      71.0       2.4
      72.0       1.0
      83.0       1.6
      84.0       2.4
      85.0       1.0
      98.0       3.1
     112.0       2.4
     184.0       4.1
     185.0       2.3
     186.0       1.7
     196.0      15.8
     197.0       2.4
     198.0     100.0
     199.0      14.8
     200.0       1.0
     211.0       2.1
     212.0       2.8
     224.0       1.6
     226.0       1.9
     254.0       1.0
     352.0       3.3
     353.0       3.8
     354.0       1.0

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₂₄ H₅₁ N	0.033 g : 0.5 ml CDCl₃
didodecylamine

    Assign.     Shift(ppm)

      A             2.587
      B             1.9
      C             1.49
      D             1.29
      E             1.26
      F             0.88

     Hz     ppm     Int.

   1041.38   2.606     77
   1034.06   2.588    114
   1026.73   2.570     85
    601.44   1.505     40
    594.73   1.489     60
    587.65   1.471     47
    526.00   1.317     69
    511.60   1.281    286
    502.56   1.258   1000
    358.40   0.897    125
    351.68   0.880    376
    344.60   0.863    154

in CDCl3

KBr disc

nujol mull

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