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MS-NW-6068 N-(2-aminoethyl)piperidine C7H16N2 (Mass of molecular ion: 128)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 2.2 18.0 2.2 27.0 3.3 28.0 4.1 29.0 2.2 30.0 9.2 39.0 2.3 41.0 14.2 42.0 13.2 43.0 3.2 44.0 11.6 54.0 1.1 55.0 14.0 56.0 3.5 57.0 1.1 69.0 5.0 70.0 5.2 83.0 1.0 84.0 3.7 96.0 1.3 98.0 100.0 99.0 7.0 128.0 1.3
400 MHz in CDCl3
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1H NMR 399.65 MHz C7 H16 N2 0.05 ml : 0.5 ml CDCl3 N-(2-aminoethyl)piperidine Assign. Shift(ppm)
A 2.783 B 2.372 C 2.37 D 1.89 E 1.572 F 1.44
Hz ppm Int.
1126.34 2.819 22 1126.10 2.818 22 1118.90 2.800 324 1116.21 2.793 58 1112.55 2.784 664 1106.20 2.768 359 953.74 2.387 652 947.51 2.371 1000 941.04 2.355 484 753.54 1.886 449 634.40 1.588 365 628.66 1.574 531 623.05 1.559 448
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