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MS-KW-0084 2-butoxypyridine C9H13NO (Mass of molecular ion: 151)
Source Temperature: 230 °C Sample Temperature: 150 °C Reservoir, 75 eV
27.0 6.7 28.0 4.8 29.0 10.7 38.0 1.8 39.0 11.5 40.0 2.6 41.0 14.9 42.0 1.0 50.0 1.4 51.0 8.4 52.0 4.6 53.0 1.8 55.0 2.7 56.0 5.0 57.0 2.0 66.0 2.5 67.0 31.4 68.0 2.2 78.0 30.8 79.0 18.8 80.0 5.1 93.0 1.8 94.0 1.1 95.0 100.0 96.0 24.3 97.0 1.6 106.0 1.9 107.0 1.0 108.0 20.2 109.0 2.7 121.0 13.7 122.0 16.1 123.0 1.3 150.0 1.3 151.0 6.2 152.0 1.2
400 MHz in CDCl3
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1H NMR 399.65 MHz C9 H13 N O 0.05 ml : 0.5 ml CDCl3 2-butoxypyridine Assign. Shift(ppm)
A 8.141 B 7.524 C 6.815 D 6.712 E 4.286 F 1.756 G 1.480 J 0.969
Hz ppm Int.
3257.69 8.152 136 3256.96 8.150 144 3255.74 8.147 148 3254.88 8.145 142 3252.69 8.139 138 3251.83 8.137 147 3250.61 8.134 146 3249.88 8.132 137 3015.99 7.547 144 3014.04 7.542 143 3008.91 7.529 160 3007.69 7.526 173 3006.96 7.524 172 3005.62 7.521 159 3000.61 7.509 158 2998.54 7.503 155 2730.22 6.832 159 2729.37 6.830 168 2725.22 6.820 161 2724.24 6.817 176 2723.14 6.814 166 2722.29 6.812 161 2718.14 6.802 148 2717.16 6.799 154 2687.74 6.726 184 2686.89 6.724 299 2685.91 6.721 181 2679.32 6.705 178 2678.47 6.703 297 2677.61 6.700 175 1719.85 4.304 382 1713.13 4.287 687 1706.42 4.270 385 716.19 1.793 83 709.72 1.776 188 709.11 1.775 194 706.67 1.769 80 703.25 1.760 192 702.27 1.758 238 701.17 1.755 149 699.95 1.752 145 696.53 1.743 86 694.34 1.738 212 687.74 1.721 99 609.62 1.526 55 604.00 1.512 47 602.29 1.508 166 596.56 1.493 102 594.60 1.488 232 589.11 1.475 102 587.04 1.469 239 581.79 1.456 45 579.71 1.451 158 572.39 1.433 49 394.41 0.987 571 387.08 0.969 1000 379.64 0.950 493
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