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BIS[4-(2-HYDROXYETHOXY)PHENYL] SULFONE

Product Name BIS[4-(2-HYDROXYETHOXY)PHENYL] SULFONE

CAS27205-03-4

MFC16H18O6S

MW338.38

¹³CNMR

Mass

MS-IW-4875          
2,2'-(sulfonylbis(p-phenyleneoxy))diethanol
C16H18O6S           (Mass of molecular ion:    338)

   Source Temperature: 180 °C
   Sample Temperature: 190 °C
   Direct, 75 eV

      18.0       2.3
      19.0       2.4
      27.0       3.8
      28.0       1.0
      29.0       2.3
      31.0       1.3
      39.0       4.1
      43.0       2.8
      44.0       1.6
      45.0      36.2
      50.0       2.1
      51.0       1.3
      53.0       1.3
      55.0       1.2
      63.0       3.2
      64.0       2.6
      65.0      13.8
      66.0       1.2
      70.0       1.0
      75.0       1.9
      76.0       4.9
      77.0       2.9
      78.0       1.2
      79.0       1.1
      81.0       2.6
      85.0       1.1
      91.0       1.1
      92.0       1.2
      93.0      12.2
      94.0      10.8
      95.0       1.6
      96.0       1.1
      97.0       1.0
     106.0       1.0
     107.0       1.6
     109.0      25.0
     110.0      44.4
     111.0       3.1
     113.0       1.2
     115.0       1.0
     119.0       1.1
     120.0       1.3
     121.0       1.3
     124.0       2.1
     125.0       2.2
     128.0       1.2
     137.0       6.5
     138.0       1.3
     139.0       1.9
     141.0      49.2
     142.0      28.8
     143.0       4.4
     144.0       1.5
     151.0       1.0
     153.0       5.9
     154.0       2.7
     157.0      20.8
     158.0       2.4
     159.0       1.2
     168.0       1.5
     169.0       1.3
     185.0      12.5
     186.0       5.8
     187.0       1.3
     201.0      16.7
     202.0       1.9
     203.0       1.3
     233.0       1.1
     249.0       1.0
     250.0      25.3
     251.0       6.0
     252.0       1.9
     263.0       2.6
     294.0      22.3
     295.0       6.0
     296.0       1.9
     307.0       2.2
     338.0     100.0
     339.0      19.5
     340.0       7.4
     341.0       1.1

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₁₆ H₁₈ O₆ S	0.039 g : 0.5 ml DMSO-d₆
2,2'-(sulfonylbis(p-phenyleneoxy))diethanol

    Assign.     Shift(ppm)

      A             7.843
      B             7.122
      C             4.93
      D             4.071
      E             3.729

     Hz     ppm     Int.

   3142.33   7.863    113
   3139.40   7.856    946
   3137.33   7.851    284
   3132.45   7.838    315
   3130.37   7.833   1000
   3127.44   7.826    114
   2853.76   7.141    127
   2850.83   7.134    958
   2848.75   7.129    287
   2843.87   7.116    296
   2841.80   7.111    897
   2838.75   7.104    104
   1976.93   4.947    240
   1971.44   4.933    590
   1966.06   4.920    250
   1632.20   4.085    417
   1627.44   4.073    649
   1622.44   4.060    468
   1497.56   3.748    229
   1492.31   3.735    497
   1487.67   3.723    455
   1482.42   3.710    200

in DMSO-d6

KBr disc

nujol mull

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