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MassMS-NW-7332 8-bromo-1-octene C8H15Br (Mass of molecular ion: 190)
Source Temperature: 210 °C Sample Temperature: 190 °C Reservoir, 75 eV
26.0 1.1 27.0 15.4 28.0 2.9 29.0 11.1 38.0 1.1 39.0 22.4 40.0 4.0 41.0 71.7 42.0 14.6 43.0 10.2 51.0 1.9 52.0 1.1 53.0 7.7 54.0 11.6 55.0 66.6 56.0 14.5 57.0 2.4 65.0 1.2 67.0 15.8 68.0 14.4 69.0 100.0 70.0 7.3 79.0 1.0 81.0 7.0 82.0 7.3 83.0 18.2 84.0 2.2 93.0 1.0 95.0 1.4 107.0 5.6 109.0 5.6 111.0 3.0 120.0 1.9 121.0 1.4 122.0 1.9 123.0 1.1 134.0 1.9 135.0 4.2 136.0 1.9 137.0 4.0 148.0 40.1 149.0 3.1 150.0 38.8 151.0 3.0 162.0 2.7 164.0 2.5
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H15 Br 0.05 ml : 0.5 ml CDCl3 8-bromo-1-octene 
Assign. Shift(ppm)
A 5.785 B 4.99 C 4.93 D 3.395 E 2.14 to 1.71 F 1.56 to 1.24
Hz ppm Int.540.50 6.036 55 533.94 5.962 111 530.44 5.923 71 527.38 5.889 69 523.94 5.851 148 523.31 5.844 112 517.50 5.779 105 516.69 5.770 183 513.31 5.732 113 510.19 5.697 108 506.81 5.659 217 500.38 5.588 117 457.69 5.111 108 456.19 5.094 201 455.25 5.084 219 454.69 5.077 178 453.88 5.068 337 452.44 5.052 180 448.69 5.010 183 447.50 4.997 313 446.31 4.984 248 445.19 4.971 183 444.06 4.959 106 442.06 4.936 45 440.44 4.918 85 438.94 4.902 217 437.56 4.886 360 436.69 4.876 379 435.31 4.861 246 434.00 4.846 69 311.06 3.474 412 304.44 3.400 1000 300.25 3.353 84 297.69 3.324 593 186.94 2.088 224 180.38 2.015 282 173.88 1.942 233 166.44 1.859 256 159.81 1.785 225 123.56 1.380 923
in CDCl3
liquid film
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