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MS-NW-8873 1-ethyl-2-pyrrolidinone C6H11NO (Mass of molecular ion: 113)
Source Temperature: 270 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 3.7 18.0 1.2 26.0 2.7 27.0 14.4 28.0 30.5 29.0 11.4 30.0 12.0 34.5 1.0 39.0 9.4 40.0 4.2 41.0 40.6 42.0 31.3 43.0 21.0 44.0 9.4 54.0 3.1 55.0 5.1 56.0 13.9 57.0 12.5 58.0 16.0 68.0 7.2 69.0 27.5 70.0 66.1 71.0 4.9 84.0 14.8 85.0 11.2 86.0 2.1 98.0 100.0 99.0 6.1 112.0 16.7 113.0 83.4 114.0 8.0
90 MHz in CDCl3
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1H NMR 89.56 MHz C6 H11 N O 0.04 ml : 0.5 ml CDCl3 1-ethyl-2-pyrrolidinone Assign. Shift(ppm)
A 3.39 B 3.34 C 2.36 D 2.032 E 1.122
Hz ppm Int.
310.81 3.471 181 309.75 3.459 103 303.50 3.389 284 302.38 3.377 303 300.19 3.352 49 298.63 3.335 54 297.13 3.318 202 295.06 3.295 289 287.94 3.216 99 222.38 2.484 44 220.06 2.458 66 216.69 2.420 30 214.88 2.400 51 213.06 2.379 159 205.50 2.295 167 195.19 2.180 73 193.44 2.160 74 188.06 2.100 119 187.00 2.088 151 185.56 2.072 32 184.94 2.065 39 183.94 2.054 39 180.56 2.017 187 177.50 1.982 75 174.19 1.945 48 173.19 1.934 88 171.19 1.912 38 170.50 1.904 54 107.44 1.200 474 105.56 1.179 32 100.25 1.120 1000 92.94 1.038 398
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