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MassMS-NW-8628 4-chlorobutyl phenyl ether C10H13ClO (Mass of molecular ion: 184)
Source Temperature: 260 °C Sample Temperature: 140 °C Reservoir, 75 eV
27.0 7.9 28.0 1.5 29.0 9.8 38.0 1.5 39.0 12.8 40.0 2.4 41.0 3.4 49.0 1.3 50.0 2.2 51.0 8.2 53.0 2.5 55.0 29.7 56.0 1.3 63.0 4.1 64.0 1.1 65.0 10.2 66.0 10.7 77.0 12.4 78.0 1.2 79.0 1.6 91.0 33.2 92.0 1.7 93.0 11.1 94.0 100.0 95.0 7.0 107.0 2.4 184.0 9.1 185.0 1.0 186.0 3.0
90 MHz in CDCl3
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1H NMR 89.56 MHz C10 H13 Cl O 0.05 ml : 0.5 ml CDCl3 4-chlorobutyl phenyl ether 
Assign. Shift(ppm)
A 7.248 B 6.91 C 6.87 D 3.949 E 3.575 F 2.06 to 1.80 B AND C WERE CONFIRMED BY LAOCN PROGRAM.
Hz ppm Int.661.44 7.386 42 659.19 7.361 162 658.25 7.350 162 657.31 7.340 96 656.31 7.329 111 652.06 7.281 254 650.69 7.266 442 648.25 7.239 124 647.63 7.232 117 645.19 7.204 220 643.31 7.184 479 640.38 7.151 99 638.31 7.128 37 627.63 7.008 131 626.19 6.992 220 625.13 6.981 236 621.44 6.939 236 619.44 6.917 1000 618.25 6.904 499 617.50 6.895 498 615.50 6.873 116 612.88 6.844 284 611.75 6.831 279 610.88 6.821 443 606.88 6.777 57 359.69 4.017 224 358.25 4.001 164 356.81 3.985 206 353.81 3.951 632 352.19 3.933 236 351.25 3.922 233 348.06 3.887 234 346.13 3.865 61 345.00 3.853 47 326.63 3.648 194 324.69 3.626 142 323.25 3.610 219 322.38 3.600 234 320.31 3.577 683 318.56 3.557 193 317.31 3.543 199 315.75 3.526 175 314.13 3.508 255 308.63 3.447 31 187.56 2.095 39 185.88 2.076 35 182.81 2.042 85 179.06 2.000 238 178.25 1.991 263 175.13 1.956 599 172.31 1.924 778 168.94 1.887 530 166.06 1.855 290 162.06 1.810 85 158.63 1.772 47 157.56 1.760 46
in CDCl3
liquid film
4880 A,200 M,liquid
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