3,3,5,5-TETRAMETHYLCYCLOHEXANOL

Mass

MS-IW-0568          
3,3,5,5-tetramethylcyclohexanol
C10H20O             (Mass of molecular ion:    156)

   Source Temperature: 260 °C
   Sample Temperature: 130 °C
   Reservoir, 75 eV

      27.0       4.3
      28.0       1.3
      29.0      11.8
      39.0       5.4
      40.0       1.1
      41.0      24.4
      42.0       1.5
      43.0      13.7
      44.0       2.7
      45.0       1.6
      53.0       3.2
      55.0      20.3
      56.0      25.3
      57.0      44.8
      58.0       2.5
      59.0       3.5
      67.0       9.1
      68.0       2.2
      69.0       8.3
      70.0       2.5
      71.0       5.1
      79.0       1.7
      81.0      23.0
      82.0      13.6
      83.0       8.3
      84.0       1.0
      85.0      26.5
      86.0       1.5
      95.0       8.5
      96.0       3.0
      97.0      16.1
      98.0       1.3
      99.0       1.2
     109.0       6.1
     110.0       4.2
     123.0     100.0
     124.0      10.4
     138.0       4.2

Assign. Shift(ppm) A 3.914 B 1.736 C 1.54 D 1.213 E 1.05 F 1.012 G 1.00 J 0.931 ASSIGNED BY CH-COSY

     Hz     ppm     Int.

   1564.33   3.915     39
    703.37   1.760     47
    702.03   1.757     47
    701.29   1.755     53
    700.07   1.752     46
    699.22   1.750     52
    697.88   1.747     46
    697.27   1.745     52
    691.89   1.732     32
    690.67   1.729     55
    689.94   1.727     52
    688.60   1.724     59
    686.65   1.719     56
    684.69   1.714     49
    616.82   1.544     77
    493.16   1.234     49
    481.45   1.205     42
    479.49   1.200     73
    477.42   1.195     38
    425.42   1.065     81
    411.74   1.031    136
    404.54   1.013    797
    400.88   1.004    118
    400.27   1.002    119
    396.36   0.992     37
    388.55   0.973     60
    387.94   0.971     57
    372.07   0.931   1000
    359.50   0.900     37