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N-(2-CHLOROETHYL)BENZAMIDE

Product Name N-(2-CHLOROETHYL)BENZAMIDE

CAS26385-07-9

MFC9H10ClNO

MW183.63

¹³CNMR

Mass

MS-NW-8077          
N-(2-chloroethyl)benzamide
C9H10ClNO           (Mass of molecular ion:    183)

   Source Temperature: 140 °C
   Sample Temperature: 100 °C
   Direct, 75 eV

      27.0       1.8
      28.0       1.1
      36.0       2.5
      38.0       1.0
      50.0       3.5
      51.0      11.1
      63.0       1.1
      74.0       1.0
      75.0       1.0
      76.0       2.2
      77.0      37.1
      78.0       3.0
     104.0       1.2
     105.0     100.0
     106.0       7.8
     117.0       8.6
     118.0       1.1
     121.0       1.9
     134.0       9.3
     147.0       6.8
     148.0       5.6
     182.0       2.1
     183.0      20.4
     184.0       2.8
     185.0       6.7

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₉ H₁₀ Cl N O	0.031 g : 0.5 ml CDCl₃
N-(2-chloroethyl)benzamide

    Assign.     Shift(ppm)

      A             7.797
      B             7.508
      C             7.432
      D             6.84
      E             3.78
      F             3.72

     Hz     ppm     Int.

   3133.91   7.842     40
   3133.54   7.841     40
   3133.06   7.840     40
   3119.87   7.807    890
   3112.43   7.788    890
   3101.44   7.761     34
   3100.83   7.759     31
   3009.28   7.530    216
   3001.95   7.512    542
   2994.75   7.494    424
   2988.28   7.478     56
   2987.67   7.476     55
   2976.68   7.449    740
   2969.12   7.430   1000
   2961.91   7.412    413
   2954.71   7.394     37
   2732.18   6.837    189
   1537.96   3.849     30
   1536.74   3.846     31
   1533.69   3.838     40
   1532.84   3.836     43
   1531.49   3.833     46
   1515.75   3.793    617
   1511.11   3.782    685
   1499.76   3.753    149
   1491.09   3.731    731
   1486.45   3.720    907
   1481.45   3.707    413
   1472.78   3.686     38
   1470.58   3.680     31
   1470.09   3.679     30
   1469.73   3.678     30

in CDCl3

KBr disc

nujol mull

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