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trans-1,4-Diaminocyclohexane

Product Name trans-1,4-Diaminocyclohexane

CAS2615-25-0

MFC6H14N2

MW114.19

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  • Mass

    MS-IW-8185          
    trans-1,4-cyclohexanediamine
    C6H14N2             (Mass of molecular ion:    114)
    

       Source Temperature: 220 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          18.0       5.6
          27.0       1.8
          28.0       7.2
          29.0       1.7
          30.0       7.2
          39.0       2.0
          41.0      10.0
          42.0       8.1
          43.0      46.0
          44.0       9.4
          53.0       1.1
          54.0       2.7
          55.0       2.0
          56.0      23.4
          57.0      21.0
          58.0     100.0
          59.0       4.9
          67.0       1.5
          68.0       9.5
          69.0       6.5
          70.0       2.1
          71.0       1.7
          77.0       2.3
          79.0       3.7
          80.0       1.9
          81.0       2.9
          82.0       9.0
          84.0       1.1
          85.0       2.2
          96.0      10.5
          97.0      29.0
          98.0       5.6
         115.0       2.6
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C6 H14 N2 0.036 g : 0.5 ml DMSO-d6
    trans-1,4-cyclohexanediamine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 2.432 B 1.9 C 1.67 D 0.99

         Hz     ppm     Int.
    

        983.64   2.462    118
        980.71   2.454    176
        980.22   2.453    175
        977.17   2.446    237
        973.51   2.436    329
        970.09   2.428    388
        966.67   2.419    338
        963.01   2.410    263
        959.72   2.402    196
        956.67   2.394    136
        683.59   1.711    139
        682.37   1.708    141
        677.00   1.694    210
        673.71   1.686    620
        670.29   1.678    935
        664.31   1.663   1000
        662.60   1.658    746
        660.89   1.654    680
        657.35   1.645    233
        652.10   1.632    169
        651.37   1.630    168
        416.02   1.041    140
        404.66   1.013    760
        401.61   1.005    447
        395.63   0.990    960
        394.17   0.987    988
        388.31   0.972    436
        385.01   0.964    684
        373.66   0.935    121
    

in DMSO-d6



KBr disc



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