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25791-20-2More Spectrum > (1-TETRADECYL)TRIPHENYLPHOSPHONIUM BROMIDE(25791-20-2)IR2
(1-TETRADECYL)TRIPHENYLPHOSPHONIUM BROMIDE
Product Name (1-TETRADECYL)TRIPHENYLPHOSPHONIUM BROMIDE
CAS25791-20-2
MFC32H44BrP
MW539.57
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MS-IW-6516 triphenyl(tetradecyl)phosphonium bromide C32H44BrP (Mass of molecular ion: 538)
Source Temperature: 210 °C Sample Temperature: 280 °C Direct, 75 eV
27.0 4.5 28.0 5.9 29.0 8.3 39.0 5.4 41.0 22.5 42.0 7.3 43.0 32.6 44.0 1.2 50.0 1.2 51.0 4.2 53.0 1.9 54.0 4.1 55.0 34.7 56.0 22.2 57.0 33.1 58.0 1.4 63.0 1.1 65.0 1.6 67.0 4.8 68.0 3.7 69.0 29.6 70.0 20.8 71.0 15.8 77.0 3.2 78.0 2.4 79.0 2.3 80.0 6.8 81.0 2.9 82.0 6.4 83.0 21.0 84.0 10.8 85.0 8.4 91.0 1.3 96.0 2.0 97.0 13.9 98.0 5.3 99.0 1.6 107.0 13.2 108.0 42.4 109.0 3.7 111.0 5.4 112.0 2.7 115.0 3.0 125.0 1.8 126.0 1.5 128.0 1.2 131.0 2.2 133.0 2.9 135.0 6.7 137.0 6.6 139.0 1.6 141.0 1.4 149.0 1.4 151.0 1.8 152.0 8.6 153.0 2.1 154.0 2.1 157.0 3.9 170.0 2.6 181.0 1.3 183.0 76.0 184.0 18.4 185.0 12.7 186.0 3.8 196.0 3.0 199.0 2.4 200.0 1.3 201.0 1.0 261.0 20.6 262.0 100.0 263.0 19.7 264.0 1.8 277.0 4.1 278.0 1.4
400 MHz in CDCl3
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1H NMR 399.65 MHz C32 H44 Br P 0.042 g : 0.5 ml CDCl3 triphenyl(tetradecyl)phosphonium bromide Assign. Shift(ppm)
A 7.85 B 7.82 C 7.72 D 3.72 E 1.628 F 1.24 G 1.19 J 0.869
Hz ppm Int.
3147.46 7.876 58 3145.51 7.871 308 3144.41 7.868 436 3142.94 7.865 220 3139.40 7.856 147 3137.33 7.851 613 3135.86 7.847 552 3131.84 7.837 652 3130.25 7.833 272 3128.05 7.827 154 3125.37 7.821 778 3123.54 7.816 1000 3119.63 7.806 197 3118.29 7.803 286 3117.43 7.801 283 3116.33 7.798 229 3114.87 7.794 104 3097.66 7.751 435 3096.19 7.748 267 3094.85 7.744 364 3094.24 7.743 404 3092.41 7.738 228 3091.19 7.735 348 3089.97 7.732 587 3088.38 7.728 348 3087.16 7.725 600 3085.45 7.721 289 3082.76 7.714 232 3081.67 7.711 172 3080.93 7.710 154 3080.08 7.707 122 3079.22 7.705 192 3078.25 7.703 150 1499.15 3.752 44 1491.70 3.733 71 1489.14 3.727 73 1486.69 3.720 84 1484.38 3.715 83 1480.71 3.706 74 1471.80 3.683 52 652.71 1.634 251 648.93 1.624 262 520.51 1.303 46 495.36 1.240 758 484.25 1.212 388 476.81 1.194 792 354.37 0.887 259 347.53 0.870 809 340.58 0.853 315
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