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256-96-2

Iminostilbene

Product Name Iminostilbene

CAS256-96-2

MFC14H11N

MW193.24

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  • 256-96-2_ms
    Mass 

    MS-NW-8234          
5H-dibenz(b,f)azepine
C14H11N             (Mass of molecular ion:    193)


       Source Temperature: 160 °C
   Sample Temperature: 110 °C
   Direct, 75 eV


          63.0       1.3
      81.5       1.0
      82.0       1.4
      82.5       1.8
      83.5       5.0
      89.0       1.6
      90.0       1.1
      95.5       5.1
      96.0       1.3
      96.5       6.3
      97.0       1.0
     139.0       1.8
     140.0       1.3
     163.0       1.9
     164.0       2.5
     165.0      11.5
     166.0       4.3
     167.0       5.4
     177.0       1.0
     178.0       1.0
     190.0       5.4
     191.0      12.0
     192.0      21.9
     193.0     100.0
     194.0      15.6
     195.0       1.4

400 MHz in DMSO-d6

90 MHz in DMSO-d6

  • 256-96-2_1hnmr_2

    1H NMR 399.65 MHz
    C14 H11 N 0.049 g : 0.5 ml DMSO-d6
    5H-dibenz(b,f)azepine
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             6.959
      B             6.93
      C             6.732
      D             6.685
      E             6.621
      F             6.069
     
     90MHZ : HSP-04-955
  

         Hz     ppm     Int.


       2790.53   6.983    154
   2788.70   6.978    181
   2782.59   6.963    276
   2781.49   6.960    301
   2775.39   6.945    207
   2773.68   6.941    245
   2769.65   6.931    252
   2700.07   6.757     30
   2696.66   6.748    186
   2695.07   6.744    232
   2689.21   6.729    402
   2687.62   6.725    402
   2678.34   6.702    264
   2677.37   6.700    318
   2671.14   6.684    311
   2670.04   6.681    366
   2663.70   6.666    132
   2662.72   6.663    151
   2649.54   6.630    377
   2641.60   6.610    333
   2425.54   6.070   1000

  • 256-96-2_1hnmr

    1H NMR 89.56 MHz
    C14 H11 N 0.042 g : 0.5 ml DMSO-d6
    5H-dibenz(b,f)azepine
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             6.94
      B             6.90
      C             6.73
      D             6.69
      E             6.063
     
     400MHZ : HSP-42-304
     CONFIRMED BY LAOCN PROGRAM.
  

         Hz     ppm     Int.


        632.24   7.060     98
    630.96   7.046     30
    630.62   7.042     30
    628.99   7.024    112
    627.97   7.012     44
    626.43   6.995    135
    624.72   6.976    161
    623.69   6.964    138
    622.41   6.950    144
    620.96   6.934    185
    618.74   6.909    331
    615.66   6.875    334
    611.56   6.829     61
    610.28   6.815     54
    606.95   6.778    110
    603.87   6.743    194
    602.50   6.728    753
    601.65   6.718    597
    599.51   6.694    338
    596.95   6.666    406
    596.35   6.659    454
    595.75   6.652    416
    595.07   6.645    432
    590.80   6.597     65
    588.23   6.569    238
    543.12   6.065   1000
    537.90   6.007     34

DMSO-d6

  • 256-96-2_13cnmr

KBr disc

  • 256-96-2_ir1_2

nujol mull

  • 256-96-2_ir2

  • 256-96-2_raman

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