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ETHYL 5-(CHLOROMETHYL)-2-FURANCARBOXYLATE

Product Name ETHYL 5-(CHLOROMETHYL)-2-FURANCARBOXYLATE

CAS2528-00-9

MFC8H9ClO3

MW188.61

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  • Mass 

    MS-IW-9445          
ethyl 5-chloromethyl-2-furoate
C8H9ClO3            (Mass of molecular ion:    188)


       Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV


          26.0       4.1
      27.0       8.6
      28.0       4.2
      29.0      11.2
      36.0       3.4
      37.0       1.0
      38.0       2.6
      39.0       2.0
      41.0       1.2
      43.0       1.6
      44.0       2.0
      45.0       3.5
      49.0       1.9
      50.0       4.7
      51.0      15.8
      52.0      16.1
      53.0       4.1
      69.0       1.9
      79.0      12.3
      80.0      10.4
      81.0       5.7
      87.0       2.5
      95.0       4.4
      97.0       8.3
     108.0      11.3
     109.0       4.4
     115.0       1.4
     125.0      52.2
     126.0       4.2
     143.0      30.1
     144.0       4.0
     145.0      10.1
     146.0       1.3
     153.0     100.0
     154.0       9.4
     155.0       1.0
     160.0       3.7
     162.0       1.3
     188.0      15.6
     189.0       1.5
     190.0       5.1

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C8 H9 Cl O3 0.05 ml : 0.5 ml CDCl3
    ethyl 5-chloromethyl-2-furoate
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             7.127
      B             6.505
      C             4.615
      D             4.369
      E             1.378
  

         Hz     ppm     Int.


       2850.34   7.133    307
   2846.80   7.124    303
   2601.56   6.510    287
   2598.02   6.501    273
   1844.36   4.615    844
   1757.08   4.397    201
   1750.00   4.379    549
   1742.80   4.361    553
   1735.72   4.344    201
    558.11   1.397    586
    555.54   1.391     35
    551.03   1.379   1000
    543.82   1.361    563

in CDCl3



liquid film



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