3-fluorosulphonylbenzenesulphonyl chloride

Mass

MS-IW-0745          
m-benzenedisulfonyl chloride fluoride
C6H4ClFO4S2         (Mass of molecular ion:    258)

   Source Temperature: 190 °C
   Sample Temperature: 160 °C
   Direct, 75 eV

      28.0       1.3
      36.0       1.6
      38.0       1.2
      39.0       1.1
      48.0       1.6
      50.0      10.6
      51.0       2.0
      52.0       1.1
      63.0       3.3
      64.0       7.8
      65.0       2.3
      69.0       1.3
      74.0       4.5
      75.0      19.4
      76.0       9.8
      77.0       2.9
      80.0       2.1
      83.0       3.5
      91.0       1.5
      92.0      31.9
      93.0       3.9
      95.0       6.3
      96.0       1.1
      99.0       1.7
     108.0       1.1
     111.0       2.5
     159.0      73.9
     160.0       8.4
     161.0       4.1
     175.0       1.4
     194.0       2.0
     207.0       1.8
     223.0     100.0
     224.0       8.5
     225.0      10.1
     258.0       6.7
     260.0       2.9

Assign. Shift(ppm) A 8.653 B 8.49 C 8.42 D 8.052

     Hz     ppm     Int.

    776.81   8.674    485
    775.25   8.657   1000
    773.44   8.637    698
    770.75   8.606    103
    768.44   8.581     82
    764.06   8.532    429
    762.63   8.516    284
    760.06   8.487    364
    758.00   8.464    580
    756.69   8.449    741
    754.81   8.428    501
    752.00   8.397    599
    750.44   8.380    661
    745.50   8.325     66
    744.94   8.318     58
    744.56   8.314     52
    744.19   8.310     52
    743.00   8.297     43
    742.25   8.288     40
    731.44   8.168     43
    727.56   8.124    515
    724.44   8.089     75
    724.00   8.084     72
    719.63   8.036    621
    716.69   8.003     82
    716.25   7.998     83
    715.13   7.985     68
    714.81   7.982     69
    714.44   7.978     68
    713.94   7.972     73
    711.75   7.948    237