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N-(2-FLUORENYL)PHTHALAMICACID

Product Name N-(2-FLUORENYL)PHTHALAMICACID

CAS2485-10-1

MFC21H15NO3

MW329.3487

Mass

MS-NW-2373          
N-(2-fluorenyl)phthalamic acid
C21H15NO3           (Mass of molecular ion:    329)

   Source Temperature: 230 °C
   Sample Temperature: 210 °C
   Direct, 75 eV

      17.0       4.4
      18.0      21.9
      27.0       1.3
      28.0      11.2
      32.0       1.3
      37.0       1.4
      38.0       2.5
      39.0       2.1
      44.0       2.2
      50.0      12.2
      51.0       3.0
      52.0       1.9
      62.0       1.4
      63.0       4.1
      74.0       4.7
      75.0       6.3
      76.0      34.1
      76.5       1.0
      77.0       6.2
      78.0       1.1
      87.0       1.4
      89.0       1.8
      89.5       1.7
      90.0       6.0
      90.5       4.5
      91.0       1.1
     101.0       1.1
     102.0       1.6
     103.0       1.8
     104.0      26.9
     105.0       4.6
     113.0       1.7
     115.0       1.5
     126.0       2.3
     127.0       5.0
     127.5       1.0
     128.0       1.2
     130.0       3.3
     133.5       1.4
     139.0       2.3
     140.5       1.0
     141.5       1.4
     148.0       4.7
     149.0       1.1
     150.0       2.8
     151.0       7.2
     152.0      12.1
     153.0       5.6
     154.0       1.2
     154.5       1.1
     155.5       9.0
     156.0       2.2
     162.0       1.0
     163.0      15.4
     164.0      71.9
     165.0      32.2
     166.0       4.9
     177.0       4.2
     178.0       3.7
     179.0       1.8
     180.0      39.6
     181.0      66.0
     182.0       9.9
     190.0       2.6
     191.0       1.1
     206.0       2.8
     207.0       1.5
     223.0       1.0
     226.0       1.1
     239.0       1.5
     253.0       1.8
     254.0       3.6
     255.0       1.1
     264.0       1.5
     265.0       1.2
     266.0       3.2
     267.0       5.3
     268.0       1.2
     282.0       5.7
     283.0       2.4
     310.0       5.3
     311.0     100.0
     312.0      23.7
     313.0       3.3

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₂₁ H₁₅ N O₃	saturated in DMSO-d₆
N-(2-fluorenyl)phthalamic acid

    Assign.     Shift(ppm)

      A            10.5
      B             8.059
      C     *1      7.897
      D             7.838
      E     *1      7.832
      F             7.66
      G             7.57
      J     *2      7.362
      K     *2      7.279
      L             3.928

     Hz     ppm     Int.

   4179.86  10.459    424
   3221.17   8.060    507
   3220.62   8.059    511
   3159.99   7.907    348
   3152.66   7.889    363
   3152.30   7.888    363
   3137.28   7.851    461
   3134.16   7.843    406
   3129.03   7.830    575
   3126.65   7.824    421
   3075.92   7.697    142
   3074.63   7.694    140
   3068.41   7.678    346
   3059.43   7.656    477
   3057.23   7.650    343
   3050.45   7.633    291
   3048.81   7.629    297
   3041.11   7.610    279
   3033.24   7.590    481
   3031.41   7.586    532
   3027.01   7.575    489
   3024.08   7.567    395
   3023.71   7.566    387
   3019.87   7.557    386
   2951.91   7.387    184
   2944.77   7.369    365
   2937.07   7.350    226
   2936.71   7.349    218
   2915.46   7.296    262
   2915.09   7.295    254
   2907.95   7.277    378
   2900.81   7.259    164
   2900.44   7.258    163
   1569.92   3.929   1000

KBr disc

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