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2,4'-DIHYDROXYDIPHENYLMETHANE
Product Name 2,4'-DIHYDROXYDIPHENYLMETHANE
CAS2467-03-0
MFC13H12O2
MW200.23
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MS-NW-9460 2,4'-methylenediphenol C13H12O2 (Mass of molecular ion: 200)
Source Temperature: 180 °C Sample Temperature: 120 °C Direct, 75 eV
18.0 2.9 27.0 1.8 39.0 4.2 50.0 1.1 51.0 4.5 52.0 1.5 53.0 2.2 55.0 5.0 63.0 3.0 64.0 1.4 65.0 2.6 66.0 1.4 75.0 1.0 76.0 4.6 77.0 10.6 78.0 5.7 79.0 3.6 82.0 2.4 89.0 1.3 90.0 1.5 90.5 1.6 91.0 3.4 94.0 31.7 95.0 2.2 100.0 2.2 105.0 1.6 106.0 2.1 107.0 100.0 108.0 7.7 115.0 4.2 127.0 2.0 128.0 3.3 131.0 1.7 139.0 1.0 141.0 2.2 151.0 1.9 152.0 8.0 153.0 6.6 154.0 1.1 157.0 1.2 165.0 2.4 169.0 1.5 171.0 1.9 181.0 9.7 182.0 2.2 183.0 4.7 197.0 1.5 199.0 8.3 200.0 52.2 201.0 7.4
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C13 H12 O2 0.033 g : 0.5 ml DMSO-d6 2,4'-methylenediphenol Assign. Shift(ppm)
A *1 9.33 B *1 9.15 C 7.01 D 6.99 E 6.98 F 6.797 G 6.69 J 6.660 K 3.745 CONFIRMED BY LAOCN PROGRAM
Hz ppm Int.
3730.62 9.335 578 3656.16 9.149 618 2805.63 7.021 571 2803.50 7.015 271 2801.21 7.010 210 2797.09 6.999 695 2793.58 6.991 667 2786.25 6.972 533 2720.03 6.807 290 2712.55 6.788 254 2682.34 6.712 176 2681.12 6.709 183 2675.02 6.694 296 2673.95 6.691 279 2667.54 6.675 227 2665.71 6.671 830 2663.57 6.665 290 2659.15 6.654 244 2657.17 6.649 727 2654.27 6.642 102 1496.73 3.746 1000
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