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MassMS2015-05118CW 2,4-dichlorobenzamide C7H5Cl2NO (Mass of molecular ion: 189)
Source Temperature: 240 °C Sample Temperature: 20 °C Direct, 70 eV
37.0 1.8 44.0 4.8 49.0 1.1 50.0 3.8 51.0 1.1 61.0 1.0 63.0 1.2 73.0 3.3 74.0 13.1 75.0 12.0 76.0 1.1 80.5 1.8 84.0 2.9 85.0 1.7 86.0 1.1 99.0 1.1 109.0 12.8 110.0 5.1 111.0 7.1 112.0 1.7 113.0 1.1 136.0 1.1 138.0 1.2 145.0 20.8 146.0 3.4 147.0 16.3 148.0 1.8 149.0 2.7 173.0 100.0 174.0 8.3 175.0 62.8 176.0 4.2 177.0 9.0 189.0 37.7 190.0 3.1 191.0 24.3 192.0 1.9 193.0 4.0
in CDCl3
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C7 H5 Cl2 N O 0.039 g : 0.5 ml DMSO-d6 2,4-dichlorobenzamide 
Assign. Shift(ppm)
A *1 7.95 B *1 7.69 C 7.663 D 7.48
Hz ppm Int.3177.86 7.952 99 3073.73 7.692 105 3063.72 7.667 311 3062.74 7.664 485 3061.40 7.661 312 2995.85 7.497 22 2992.31 7.488 26 2988.65 7.479 1000 2987.67 7.476 754
in CDCl3
in DMSO-d6
KBr disc
Nujol
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