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MassMS2014-05027CW 2,6-dibromo-4-methylphenol C7H6Br2O (Mass of molecular ion: 264)
Source Temperature: 250 °C Sample Temperature: 25 °C Direct, 70 eV
15.0 2.1 17.0 6.7 18.0 2.0 25.0 1.4 26.0 4.6 27.0 9.4 28.0 1.6 29.0 3.4 37.0 7.4 38.0 16.0 38.5 1.8 39.0 10.8 43.0 2.3 49.0 6.0 50.0 31.4 51.0 58.1 52.0 11.6 52.5 1.7 53.0 25.0 54.0 1.4 55.0 1.5 60.0 1.2 61.0 7.1 62.0 10.4 63.0 8.1 65.0 1.1 66.0 2.4 73.0 3.6 74.0 12.8 75.0 17.1 76.0 12.8 77.0 68.7 78.0 38.0 79.0 7.7 80.0 3.4 81.0 5.8 82.0 3.1 83.0 1.0 85.0 1.7 86.0 2.2 87.0 1.8 92.0 1.1 92.5 6.0 93.0 1.7 93.5 5.7 104.0 2.5 105.0 14.4 106.0 9.6 107.0 1.9 117.0 1.3 119.0 1.2 129.0 1.3 130.0 1.1 131.0 2.1 132.0 1.1 133.0 2.5 141.0 1.1 143.0 1.1 155.0 3.0 156.0 4.8 157.0 5.0 158.0 4.7 159.0 2.3 183.0 3.6 184.0 1.7 185.0 80.7 186.0 7.6 187.0 75.1 188.0 5.8 263.0 6.6 264.0 51.5 265.0 16.9 266.0 100.0 267.0 14.1 268.0 49.3 269.0 3.8
90 MHz in CDCl3
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1H NMR 89.56 MHz C7 H6 Br2 O 0.047 g : 0.5 ml CDCl3 2,6-dibromo-4-methylphenol 
Assign. Shift(ppm)
A 7.244 B 5.68 C 2.244
Hz ppm Int.649.75 7.255 257 649.06 7.248 447 648.38 7.240 430 509.00 5.684 388 201.69 2.253 590 201.00 2.245 1000 200.31 2.237 523
in CDCl3
KBr disc
nujol mull
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