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Methyl thioglycolate

Product Name Methyl thioglycolate

CAS2365-48-2

MFC3H6O2S

MW106.14

¹³CNMR

Mass

MS-NW-5854          
methyl mercaptoacetate
C3H6O2S             (Mass of molecular ion:    106)

   Source Temperature: 260 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      14.0       4.0
      15.0      27.9
      18.0       1.0
      27.0       1.0
      28.0       3.7
      29.0       6.8
      30.0       1.1
      31.0       3.9
      32.0       1.3
      33.0       4.7
      34.0       1.2
      41.0       1.1
      42.0      14.2
      43.0       3.7
      44.0       3.6
      45.0      25.1
      46.0      33.7
      47.0     100.0
      48.0       4.1
      49.0       5.0
      59.0      31.8
      60.0       1.5
      61.0       2.0
      74.0      69.2
      75.0      13.5
      76.0       3.7
      77.0       1.2
      78.0       1.0
      91.0       1.1
     106.0      62.2
     107.0       3.1
     108.0       3.1
     119.0       1.2
     178.0       1.4

parameter in CDCl3

¹H NMR	300 MHz
C₃ H₆ O₂ S	0.04 ml : 0.5 ml CDCl₃
methyl mercaptoacetate

    Parameter     ppm  Hz

      D(A)         3.751
     
      D(B)         3.275
      D(C)         2.026
       J(B,C)          8.25

     Hz     ppm     Int.

   1125.31   3.751   1000
    986.67   3.289    321
    978.43   3.261    337
    615.96   2.053     87
    607.72   2.026    157
    599.48   1.998     80

in CDCl3

liquid film

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