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N,N'-METHYLENEBISMETHACRYLAMIDE

Product Name N,N'-METHYLENEBISMETHACRYLAMIDE

CAS2359-15-1

MFC9H14N2O2

MW182.22

¹³CNMR

Mass

MS-NW-9481          
N,N'-methylenebis(methacrylamide)
C9H14N2O2           (Mass of molecular ion:    182)

   Source Temperature: 190 °C
   Sample Temperature: 110 °C
   Direct, 75 eV

      18.0       3.7
      28.0       3.3
      30.0       3.8
      39.0       8.8
      40.0       2.7
      41.0      41.0
      42.0       3.1
      43.0       1.4
      44.0       1.7
      45.0       1.1
      46.0      18.5
      55.0       1.5
      58.0       1.4
      68.0       5.7
      69.0     100.0
      70.0       7.1
      85.0       3.0
      86.0      14.5
      96.0       2.5
      97.0      17.2
      98.0       7.8
     113.0      67.2
     114.0       4.5
     182.0       2.2

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₉ H₁₄ N₂ O₂	0.030 g : 0.5 ml DMSO-d₆
N,N'-methylenebis(methacrylamide)

    Assign.     Shift(ppm)

      A             8.38
      B             5.716
      C             5.372
      D             4.568
      E             1.852
     
     J(A,D)=5.1HZ

     Hz     ppm     Int.

   3352.66   8.389     61
   3347.47   8.377    106
   3342.44   8.364     67
   2284.70   5.717    305
   2148.59   5.377    204
   2147.06   5.373    281
   2145.84   5.370    221
   1831.51   4.583    107
   1825.71   4.569    205
   1819.92   4.554    116
    740.20   1.853   1000

in DMSO-d6

KBr disc

nujol mull

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