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MassMS-NW-5569 L-2-pyrrolidinemethanol C5H11NO (Mass of molecular ion: 101)
Source Temperature: 250 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 1.5 18.0 1.8 27.0 3.9 28.0 20.3 29.0 1.5 30.0 6.3 31.0 2.8 39.0 3.8 41.0 9.7 42.0 4.1 43.0 15.0 44.0 2.0 53.0 1.2 54.0 1.6 55.0 7.4 56.0 1.8 68.0 5.6 69.0 1.2 70.0 100.0 71.0 5.6 82.0 1.0
400 MHz in CDCl3
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1H NMR 399.65 MHz C5 H11 N O 0.05 ml : 0.5 ml CDCl3 L-2-pyrrolidinemethanol 
Assign. Shift(ppm)
A 3.94 B *1 3.556 C *1 3.382 D 3.211 E *2 2.93 F *2 2.86 G 1.81 to 1.73 J 1.40
Hz ppm Int.1574.22 3.939 303 1428.71 3.575 649 1424.56 3.565 694 1417.72 3.548 868 1413.57 3.538 870 1360.47 3.405 837 1353.27 3.387 1000 1349.49 3.377 648 1342.29 3.359 758 1287.72 3.223 565 1283.57 3.212 559 1280.52 3.205 578 1276.37 3.194 516 1176.03 2.943 389 1172.12 2.933 585 1169.80 2.928 341 1165.89 2.918 766 1158.94 2.900 836 1151.49 2.882 779 1148.19 2.873 330 1144.78 2.865 511 1140.75 2.855 367 731.20 1.830 327 727.05 1.820 409 725.95 1.817 468 723.27 1.810 475 720.21 1.803 291 718.26 1.798 657 716.92 1.794 543 715.45 1.791 549 713.99 1.787 435 712.16 1.782 470 710.45 1.778 572 708.25 1.773 398 706.30 1.768 723 704.10 1.762 599 701.54 1.756 372 699.34 1.750 552 697.63 1.746 720 696.29 1.743 689 692.63 1.734 472 690.80 1.729 601 690.43 1.728 599 688.84 1.724 557 687.62 1.721 508 686.40 1.718 390 682.62 1.709 405 681.40 1.705 361 680.30 1.703 377 569.21 1.425 346 568.24 1.422 366 564.58 1.413 369 560.91 1.404 409 557.74 1.396 517 554.08 1.387 283 550.54 1.378 358
in CDCl3
liquid film
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