1,1'-Bi(cycloheptane)

Mass

MS-IW-1709          
bicycloheptyl
C14H26              (Mass of molecular ion:    194)

   Source Temperature: 270 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV

      27.0       2.4
      29.0       4.2
      39.0       4.2
      41.0      15.9
      42.0       1.7
      43.0       4.2
      53.0       3.2
      54.0       8.5
      55.0      79.1
      56.0       4.4
      65.0       1.0
      66.0       3.4
      67.0      24.1
      68.0      13.2
      69.0      10.2
      70.0       1.3
      71.0       3.4
      77.0       1.3
      79.0       2.3
      81.0      38.3
      82.0       6.0
      83.0       2.9
      91.0       1.3
      95.0       5.9
      96.0     100.0
      97.0      74.0
      98.0       5.4
     104.0       1.3
     109.0       1.2
     110.0       1.5
     123.0       1.0
     194.0       2.4

Assign. Shift(ppm) A *1 1.661 B *2 1.59 C *3 1.53 D *3 1.46 E 1.38 F *1 1.38 G *2 1.249 ASSIGNED BY H-H COSY

     Hz     ppm     Int.

    690.43   1.728     32
    688.60   1.724     37
    686.40   1.718     54
    681.40   1.705    101
    678.71   1.699    226
    677.37   1.695    192
    675.17   1.690    301
    671.88   1.682    430
    668.46   1.673    476
    665.16   1.665    387
    661.99   1.657    486
    658.94   1.649    450
    655.40   1.640    422
    652.10   1.632    353
    648.80   1.624    252
    634.77   1.589    565
    630.86   1.579    579
    627.32   1.570    665
    624.15   1.562    844
    621.58   1.556    732
    620.24   1.552    725
    617.43   1.545   1000
    613.65   1.536    727
    612.06   1.532    613
    607.91   1.522    405
    607.06   1.519    336
    602.78   1.509    130
    600.46   1.503    143
    594.60   1.488    373
    590.82   1.479    386
    586.43   1.468    512
    585.21   1.465    499
    581.79   1.456    480
    578.49   1.448    346
    577.03   1.444    282
    576.29   1.442    287
    574.83   1.439    487
    571.53   1.431    454
    568.73   1.424    408
    565.19   1.415    445
    563.23   1.410    439
    561.16   1.405    303
    559.81   1.401    363
    558.72   1.399    344
    556.27   1.392    629
    552.98   1.384    505
    549.56   1.376    369
    546.63   1.368    649
    543.46   1.360    680
    540.04   1.352    317
    538.21   1.347    304
    537.35   1.345    317
    535.03   1.339    414
    534.30   1.337    433
    532.23   1.332    365
    529.30   1.325    158
    523.32   1.310     52
    523.07   1.309     52
    514.28   1.287    403
    510.74   1.278    373
    504.64   1.263    420
    501.22   1.255    628
    497.80   1.246    326
    495.00   1.239    269
    491.46   1.230    484
    487.92   1.221    317
    481.69   1.206    175
    478.15   1.197    124