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3-Hydroxy-2-iodo-6-methylpyridine

Product Name 3-Hydroxy-2-iodo-6-methylpyridine

CAS23003-30-7

MFC6H6INO

MW235.02

¹³CNMR

Mass

MS-IW-0563          
2-iodo-6-methyl-3-pyridinol
C6H6INO             (Mass of molecular ion:    235)

   Source Temperature: 270 °C
   Sample Temperature: 130 °C
   Reservoir, 75 eV

      26.0       2.1
      27.0      10.3
      28.0       3.5
      29.0       1.2
      31.0       1.4
      37.0       1.1
      38.0       2.2
      39.0       5.5
      40.0       1.0
      41.0       1.3
      42.0       1.2
      43.0       5.7
      44.0       1.5
      45.0       2.6
      50.0       3.1
      51.0       9.1
      52.0      17.0
      53.0      48.9
      54.0       5.0
      55.0       2.0
      63.0       1.4
      64.0       1.7
      66.0       2.7
      78.0       3.6
      79.0       7.2
      80.0      20.0
      81.0       4.8
     106.0       3.1
     107.0       8.6
     108.0      96.9
     109.0       8.2
     117.5       1.3
     127.0       3.0
     128.0       1.9
     187.0       7.5
     189.0       7.4
     235.0     100.0
     236.0       7.3

90 MHz in DMSO-d6

¹H NMR	89.56 MHz
C₆ H₆ I N O	0.042 g : 0.5 ml DMSO-d₆
2-iodo-6-methyl-3-pyridinol

    Assign.     Shift(ppm)

      A            10.51
      B             7.05
      C             2.332

     Hz     ppm     Int.

    940.97  10.507    144
    634.80   7.088     27
    631.04   7.047    807
    208.92   2.333   1000

in DMSO-d6

KBr disc

nujol mull

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