D-glucose(2280-44-6) 1H NMR

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₆ H₁₂ O₆	0.039 g : 0.5 ml DMSO-d₆
D-glucopyranose

    Assign.     Shift(ppm)

      A             6.575
      B             6.202
      C             4.91
      D             4.84
      E             4.77
      F             4.64
      G             4.48
      J             4.37
      K             4.27
      L             3.660
      M             3.57
      N             3.42
      P             3.10
      Q             3.04
      R             2.887
     
     ASSIGNED BY H-H AND C-H COSY.
     H2O PEAK AT 3.40 PPM REMOVED.

     Hz     ppm     Int.

   2630.98   6.584    703
   2624.51   6.568    718
   2481.57   6.210    169
   2480.83   6.208    182
   2477.05   6.199    181
   2476.32   6.197    170
   1964.97   4.917    102
   1960.94   4.907    153
   1956.79   4.897    107
   1937.99   4.850    848
   1936.77   4.847    836
   1934.33   4.841    803
   1933.35   4.838   1000
   1932.13   4.835    855
   1929.44   4.828    654
   1926.27   4.820     44
   1909.06   4.777    279
   1903.56   4.764    291
   1857.67   4.649    287
   1852.78   4.637    289
   1797.49   4.498    250
   1794.68   4.491     43
   1791.50   4.483    494
   1785.40   4.468    465
   1750.98   4.382     87
   1745.61   4.368    137
   1744.87   4.366    173
   1739.38   4.353    115
   1713.99   4.289    285
   1707.40   4.273    333
   1706.30   4.270    353
   1699.71   4.253    295
   1472.41   3.685    110
   1470.58   3.680    121
   1466.80   3.671    113
   1464.97   3.666    131
   1460.82   3.656    158
   1458.74   3.651    145
   1455.32   3.642    145
   1453.37   3.637    139
   1445.80   3.618     47
   1443.48   3.612     54
   1440.43   3.605     45
   1438.11   3.599     55
   1434.45   3.590     61
   1433.47   3.587     45
   1432.25   3.584     78
   1427.25   3.572    140
   1422.61   3.560     66
   1421.14   3.556     48
   1420.29   3.554     56
   1417.85   3.548     60
   1415.89   3.543     47
   1412.60   3.535     67
   1410.52   3.530     58
   1410.16   3.529     53
   1388.55   3.475     58
   1383.06   3.461     74
   1382.45   3.460     66
   1376.95   3.446    122
   1374.63   3.440    134
   1373.54   3.437    107
   1371.70   3.433     97
   1368.77   3.425    289
   1363.04   3.411    286
   1357.18   3.396    208
   1354.98   3.391    103
   1353.15   3.386     49
   1351.32   3.382    115
   1253.66   3.137     96
   1253.30   3.136     96
   1249.15   3.126    127
   1245.36   3.117    239
   1242.55   3.110    136
   1240.60   3.105    233
   1236.33   3.094    223
   1231.93   3.083    224
   1229.74   3.078     97
   1225.95   3.068    218
   1223.88   3.063    223
   1220.09   3.053    260
   1218.14   3.049    431
   1213.38   3.037    270
   1209.96   3.028    182
   1208.74   3.025    140
   1206.54   3.019     67
   1205.08   3.016    171
   1204.10   3.013    142
   1200.56   3.005     72
   1195.56   2.992     69
   1164.31   2.914    157
   1159.67   2.902    158
   1156.49   2.894    188
   1155.52   2.892    171
   1151.86   2.883    192
   1150.76   2.880    171
   1147.58   2.872    133
   1142.94   2.860    130

in D2O

in DMSO-d6

KBr disc

nujol mull