(R)-(+)-2-AMINOMETHYL-1-ETHYLPYRROLIDINE

Mass

MS-IW-7683          
(R)-(1-ethyl-2-pyrrolidinyl)methylamine
C7H16N2             (Mass of molecular ion:    128)

   Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      27.0       2.4
      28.0       9.1
      29.0       2.7
      30.0       3.7
      39.0       1.5
      41.0       5.1
      42.0       2.9
      43.0       6.8
      44.0       1.2
      54.0       1.4
      55.0       2.0
      56.0       4.3
      67.0       1.1
      68.0       4.5
      69.0       1.6
      70.0      21.2
      71.0       1.7
      80.0       1.6
      82.0       2.9
      95.0       1.0
      96.0       4.2
      97.0       1.9
      98.0     100.0
      99.0       7.5

Assign. Shift(ppm) A 3.152 B *1 2.821 C *2 2.722 D *2 2.675 E 2.367 F *1 2.205 G 2.136 J 2.05 K 1.880 L *3 1.74 M *3 1.71 P 1.604 Q 1.097 ASSIGNED BY C-H COSY

     Hz     ppm     Int.

   1269.90   3.178     62
   1264.77   3.165    106
   1260.38   3.154    119
   1255.25   3.141     99
   1251.10   3.131     71
   1145.14   2.866     36
   1137.70   2.847    106
   1133.18   2.836     48
   1130.25   2.829    112
   1125.73   2.817    119
   1122.92   2.810     48
   1118.41   2.799    119
   1110.96   2.780     43
   1099.49   2.752     77
   1095.70   2.742     88
   1086.79   2.720    228
   1082.89   2.710    238
   1075.81   2.692    214
   1069.70   2.677    228
   1062.99   2.660     72
   1057.01   2.645     86
    958.37   2.399     38
    954.59   2.389     40
    951.90   2.382     65
    950.07   2.378     59
    948.24   2.373     69
    946.04   2.368     76
    943.73   2.362     76
    942.02   2.358     55
    939.94   2.352     70
    937.50   2.346     45
    933.59   2.337     37
    897.71   2.247     47
    890.63   2.229    141
    885.74   2.217     54
    883.54   2.211    151
    878.78   2.199    136
    876.59   2.194     67
    871.70   2.182    139
    867.07   2.170     85
    864.62   2.164     58
    858.28   2.148    194
    849.73   2.127    200
    840.94   2.105    100
    819.58   2.051    240
    771.36   1.931     37
    763.43   1.911     89
    759.40   1.901     46
    755.25   1.890    112
    752.56   1.884     65
    750.85   1.879     69
    746.83   1.869     57
    743.29   1.860     84
    741.94   1.857     60
    734.86   1.839     65
    704.22   1.763     54
    701.66   1.756     56
    698.12   1.747    115
    695.92   1.742    138
    693.60   1.736     76
    691.28   1.730    144
    689.58   1.726    137
    688.60   1.724    155
    687.50   1.721    197
    682.86   1.709    214
    679.32   1.700    109
    674.56   1.688    101
    655.03   1.640     56
    650.51   1.628     36
    648.56   1.623     70
    646.73   1.619     49
    643.43   1.610     68
    640.38   1.603     49
    636.23   1.592     80
    630.98   1.579     33
    629.27   1.575     67
    445.80   1.116    610
    438.48   1.098   1000
    431.40   1.080    631