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BENZAL-P-TOLUIDINE

Product Name BENZAL-P-TOLUIDINE

CAS2272-45-9

MFC14H13N

MW195.26

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  • Mass 

    MS-NW-6241          
N-benzylidene-p-toluidine
C14H13N             (Mass of molecular ion:    195)


       Source Temperature: 260 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV


          27.0       1.3
      38.0       1.0
      39.0       7.4
      41.0       2.3
      50.0       2.2
      51.0       5.7
      52.0       1.6
      62.0       1.3
      63.0       5.4
      64.0       2.1
      65.0      17.1
      66.0       1.1
      76.0       1.5
      77.0       5.3
      78.0       4.1
      83.5       2.8
      89.0       8.1
      90.0       6.1
      91.0      36.3
      92.0       3.3
      95.5       1.5
      96.5       5.3
      97.0       1.0
     106.0       1.1
     116.0       2.3
     117.0       2.1
     118.0      13.0
     119.0       1.4
     152.0       1.6
     165.0       1.6
     167.0       1.0
     180.0       2.5
     192.0       1.1
     193.0       2.5
     194.0      79.9
     195.0     100.0
     196.0      14.9
     197.0       1.2

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C14 H13 N 0.039 g : 0.5 ml CDCl3
    N-benzylidene-p-toluidine
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             8.446
      B             7.882
      C             7.45
      D             7.181
      E             7.138
      F             2.355
  

         Hz     ppm     Int.


       3375.37   8.446    441
   3158.69   7.904     30
   3157.23   7.900     35
   3155.27   7.896    177
   3152.83   7.889    186
   3150.63   7.884    150
   3149.29   7.881    215
   3146.97   7.875    127
   3145.63   7.871    185
   2982.91   7.464     69
   2979.25   7.455    441
   2976.32   7.448    395
   2974.85   7.444    212
   2972.66   7.439    311
   2970.21   7.433     86
   2875.61   7.196    178
   2867.43   7.175    385
   2857.06   7.149    105
   2855.22   7.145    495
   2853.03   7.139    156
   2848.88   7.129     88
   2846.80   7.124    216
    941.28   2.356   1000

in CDCl3



KBr disc



liquid film



nujol mull



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