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MassMS-NW-8430 1,2-dichlorooctane C8H16Cl2 (Mass of molecular ion: 182)
Source Temperature: 260 °C Sample Temperature: 140 °C Reservoir, 75 eV
26.0 1.3 27.0 26.4 28.0 4.8 29.0 34.9 36.0 2.8 38.0 1.3 39.0 22.1 40.0 3.9 41.0 82.2 42.0 35.1 43.0 100.0 44.0 3.4 49.0 4.4 51.0 3.3 53.0 11.8 54.0 18.6 55.0 81.2 56.0 41.7 57.0 37.2 58.0 1.6 59.0 1.3 61.0 3.1 62.0 3.0 63.0 6.8 64.0 1.1 65.0 3.5 66.0 2.1 67.0 26.7 68.0 28.6 69.0 30.4 70.0 63.2 71.0 9.5 75.0 12.0 76.0 3.5 77.0 7.3 78.0 1.4 79.0 3.5 80.0 1.1 81.0 37.1 82.0 12.7 83.0 12.4 84.0 6.9 85.0 6.5 89.0 9.4 90.0 3.0 91.0 11.4 92.0 1.3 93.0 2.9 95.0 7.5 97.0 18.1 98.0 1.4 103.0 29.9 104.0 34.9 105.0 12.5 106.0 11.3 107.0 1.2 109.0 2.2 110.0 3.4 111.0 3.0 117.0 8.0 118.0 3.8 119.0 3.2 120.0 1.2 125.0 4.4 127.0 2.7 139.0 21.6 140.0 1.3 141.0 14.1 143.0 2.5 153.0 1.8 155.0 1.1
400 MHz in CDCl3
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1H NMR 399.65 MHz C8 H16 Cl2 0.05 ml : 0.5 ml CDCl3 1,2-dichlorooctane 
Assign. Shift(ppm)
A 4.036 B *1 3.760 C *1 3.657 D *2 1.985 E *2 1.712 F *3 1.55 G *3 1.41 J 1.31 K 0.894
Hz ppm Int.1625.85 4.069 64 1622.07 4.059 72 1620.73 4.056 78 1618.41 4.050 83 1616.94 4.046 137 1614.62 4.041 92 1613.28 4.037 139 1611.82 4.034 91 1609.50 4.028 150 1607.91 4.024 84 1605.71 4.018 80 1604.37 4.015 85 1600.59 4.005 76 1512.21 3.784 272 1506.96 3.771 260 1500.85 3.756 453 1495.73 3.743 403 1469.36 3.677 465 1461.91 3.658 436 1458.01 3.649 298 1450.56 3.630 263 811.16 2.030 53 807.37 2.021 58 805.79 2.017 64 801.88 2.007 68 801.15 2.005 85 797.24 1.995 136 795.41 1.991 85 793.33 1.986 85 791.50 1.981 145 786.99 1.970 115 783.08 1.960 95 781.13 1.955 95 777.34 1.946 91 703.00 1.760 61 698.49 1.748 89 693.36 1.735 97 689.45 1.726 107 688.48 1.723 130 684.33 1.713 126 679.44 1.701 130 675.42 1.691 72 674.19 1.687 82 670.04 1.677 57 665.28 1.665 74 573.36 1.435 76 568.73 1.424 73 563.11 1.410 75 554.93 1.389 75 528.56 1.323 308 527.47 1.320 323 525.76 1.316 367 521.48 1.305 632 516.60 1.293 358 364.38 0.912 298 361.94 0.906 214 361.08 0.904 232 357.54 0.895 1000 354.86 0.888 168 350.59 0.878 296
in CDCl3
liquid film
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